C₃₇H₅₆O₆Si

Base Information

Chemical Name:C₃₇H₅₆O₆Si
CAS No.:1586033-66-0
Molecular Formula:C₃₇H₅₆O₆Si
Molecular Weight:624.934
Hs Code.:

C<sub>37</sub>H<sub>56</sub>O<sub>6</sub>Si

Synonyms:C₃₇H₅₆O₆Si

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Chemical Property of C₃₇H₅₆O₆Si

Chemical Property:

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Technology Process of C₃₇H₅₆O₆Si

There total 9 articles about C₃₇H₅₆O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1586033-55-7
(S,E)-6-((4S,5S)-5-((R)-1-(tert-butyldiphenylsilyloxy)octyl)-2,2-dimethyl-1,3-dioxolan-4-yl)-4-(methoxymethoxy)hex-5-en-1-ol

: 1586033-66-0
C₃₇H₅₆O₆Si

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 0 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.tet.2014.02.072

Reference yield:

: 1586033-59-1
C₉H₁₈O₂

: 1586033-66-0
C₃₇H₅₆O₆Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: dmap; 1H-imidazole / dichloromethane / 6 h / 0 - 20 °C / Inert atmosphere

2.1: sodium hydride / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

3.1: 4-methylmorpholine N-oxide; osmium(VIII) oxide / tetrahydrofuran; water / 12 h / 20 °C / Inert atmosphere

4.1: camphorsulphonic acid / dichloromethane / 20 °C / Inert atmosphere

5.1: diisobutylaluminium hydride / dichloromethane / 2.5 h / -78 °C / Inert atmosphere

6.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

6.2: 1 h / 20 °C / Inert atmosphere

7.1: Hoveyda-Grubbs catalyst second generation / dichloromethane / 24 h / Inert atmosphere; Reflux

8.1: sodium iodide; N-ethyl-N,N-diisopropylamine / Inert atmosphere

9.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 1 h / 20 °C / Inert atmosphere

10.1: Dess-Martin periodane / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

With 1H-imidazole; dmap; osmium(VIII) oxide; Hoveyda-Grubbs catalyst second generation; sodium hydride; diisobutylaluminium hydride; Dess-Martin periodane; 4-methylmorpholine N-oxide; N-ethyl-N,N-diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium iodide; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; water; 2.1: |Horner-Wadsworth-Emmons Olefination / 2.2: |Horner-Wadsworth-Emmons Olefination / 6.1: |Wittig Olefination / 6.2: |Wittig Olefination / 7.1: |Cross Metathesis;
DOI:10.1016/j.tet.2014.02.072

Reference yield:

: 124-19-6
nonan-1-al

: 1586033-66-0
C₃₇H₅₆O₆Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: Nitrosobenzene; L-proline / dimethyl sulfoxide / 3 h / 20 °C / Inert atmosphere

1.2: 6 h / 0 °C / Inert atmosphere

2.1: dmap; 1H-imidazole / dichloromethane / 6 h / 0 - 20 °C / Inert atmosphere

3.1: sodium hydride / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

3.2: 0 - 20 °C / Inert atmosphere

4.1: 4-methylmorpholine N-oxide; osmium(VIII) oxide / tetrahydrofuran; water / 12 h / 20 °C / Inert atmosphere

5.1: camphorsulphonic acid / dichloromethane / 20 °C / Inert atmosphere

6.1: diisobutylaluminium hydride / dichloromethane / 2.5 h / -78 °C / Inert atmosphere

7.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

7.2: 1 h / 20 °C / Inert atmosphere

8.1: Hoveyda-Grubbs catalyst second generation / dichloromethane / 24 h / Inert atmosphere; Reflux

9.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 1 h / 20 °C / Inert atmosphere

10.1: Dess-Martin periodane / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

With 1H-imidazole; dmap; osmium(VIII) oxide; Hoveyda-Grubbs catalyst second generation; sodium hydride; diisobutylaluminium hydride; Dess-Martin periodane; 4-methylmorpholine N-oxide; Nitrosobenzene; 2,3-dicyano-5,6-dichloro-p-benzoquinone; L-proline; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; 3.1: |Horner-Wadsworth-Emmons Olefination / 3.2: |Horner-Wadsworth-Emmons Olefination / 7.1: |Wittig Olefination / 7.2: |Wittig Olefination / 8.1: |Cross Metathesis;
DOI:10.1016/j.tet.2014.02.072