N-(1-((4-((3-aminopropyl)amino)butyl)amino)-1-oxo-4-phenylbutan-2-yl)-7-guanidinoheptanamide

Base Information

Chemical Name:N-(1-((4-((3-aminopropyl)amino)butyl)amino)-1-oxo-4-phenylbutan-2-yl)-7-guanidinoheptanamide
CAS No.:1310012-73-7
Molecular Formula:C₂₅H₄₅N₇O₂
Molecular Weight:475.678
Hs Code.:

Synonyms:N-(1-((4-((3-aminopropyl)amino)butyl)amino)-1-oxo-4-phenylbutan-2-yl)-7-guanidinoheptanamide

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Chemical Property of N-(1-((4-((3-aminopropyl)amino)butyl)amino)-1-oxo-4-phenylbutan-2-yl)-7-guanidinoheptanamide

Chemical Property:

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Technology Process of N-(1-((4-((3-aminopropyl)amino)butyl)amino)-1-oxo-4-phenylbutan-2-yl)-7-guanidinoheptanamide

There total 9 articles about N-(1-((4-((3-aminopropyl)amino)butyl)amino)-1-oxo-4-phenylbutan-2-yl)-7-guanidinoheptanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₂H₅₁N₇O₂

: 1310012-73-7
N-(1-((4-((3-aminopropyl)amino)butyl)amino)-1-oxo-4-phenylbutan-2-yl)-7-guanidinoheptanamide

Guidance literature:: With ammonium cerium (IV) nitrate; In water; acetonitrile; for 2h;
DOI:10.1016/j.bmcl.2011.02.079

Reference yield:

: C₄₄H₆₈N₆O₈

: 1310012-73-7
N-(1-((4-((3-aminopropyl)amino)butyl)amino)-1-oxo-4-phenylbutan-2-yl)-7-guanidinoheptanamide

Guidance literature:: Multi-step reaction with 4 steps

1: phosphoric acid / N,N-dimethyl-formamide

2: sodium tris(acetoxy)borohydride / tetrahydrofuran / 1.5 h / 20 °C

3: Tris-amine resin / 0.5 h / 20 °C

4: ammonium cerium (IV) nitrate / water; acetonitrile / 2 h

With ammonium cerium (IV) nitrate; phosphoric acid; sodium tris(acetoxy)borohydride; In tetrahydrofuran; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.bmcl.2011.02.079

Reference yield:

: 104-53-0
3-phenyl-propionaldehyde

: 1310012-73-7
N-(1-((4-((3-aminopropyl)amino)butyl)amino)-1-oxo-4-phenylbutan-2-yl)-7-guanidinoheptanamide

Guidance literature:: Multi-step reaction with 5 steps

1: N,N-dimethyl-formamide / 0.33 h / 100 °C / Microwave irradiation

2: phosphoric acid / N,N-dimethyl-formamide

3: sodium tris(acetoxy)borohydride / tetrahydrofuran / 1.5 h / 20 °C

4: Tris-amine resin / 0.5 h / 20 °C

5: ammonium cerium (IV) nitrate / water; acetonitrile / 2 h

With ammonium cerium (IV) nitrate; phosphoric acid; sodium tris(acetoxy)borohydride; In tetrahydrofuran; water; N,N-dimethyl-formamide; acetonitrile; 1: Ugi reaction;
DOI:10.1016/j.bmcl.2011.02.079