N-(3,4,4a,5-Tetrahydro-3-oxo-2H-(1)benzopyrano(4,3-c)pyridazin-9-yl)acetamide

Base Information

Chemical Name:N-(3,4,4a,5-Tetrahydro-3-oxo-2H-(1)benzopyrano(4,3-c)pyridazin-9-yl)acetamide
CAS No.:133414-49-0
Molecular Formula:C₁₃H₁₃N₃O₃
Molecular Weight:259.265
Hs Code.:
DSSTox Substance ID:DTXSID20928111

Synonyms:BRN 4263735;133414-49-0;N-(3,4,4a,5-Tetrahydro-3-oxo-2H-(1)benzopyrano(4,3-c)pyridazin-9-yl)acetamide;Acetamide, N-(3,4,4a,5-tetrahydro-3-oxo-2H-(1)benzopyrano(4,3-c)pyridazin-9-yl)-;DTXSID20928111;N-(3-Hydroxy-4a,5-dihydro-4H-[1]benzopyrano[4,3-c]pyridazin-9-yl)ethanimidic acid

Suppliers and Price of N-(3,4,4a,5-Tetrahydro-3-oxo-2H-(1)benzopyrano(4,3-c)pyridazin-9-yl)acetamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of N-(3,4,4a,5-Tetrahydro-3-oxo-2H-(1)benzopyrano(4,3-c)pyridazin-9-yl)acetamide

Chemical Property:

Density:1.51g/cm³
XLogP3:-0.1
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:1
Exact Mass:259.09569129
Heavy Atom Count:19
Complexity:435

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)NC1=CC2=C(C=C1)OCC3C2=NNC(=O)C3

Technology Process of N-(3,4,4a,5-Tetrahydro-3-oxo-2H-(1)benzopyrano(4,3-c)pyridazin-9-yl)acetamide

There total 3 articles about N-(3,4,4a,5-Tetrahydro-3-oxo-2H-(1)benzopyrano(4,3-c)pyridazin-9-yl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 133414-57-0
(6-Acetylamino-4-oxo-chroman-3-yl)-acetic acid

: 133414-49-0
N-(2-Oxo-2,3,10,10a-tetrahydro-1H-9-oxa-3,4-diaza-phenanthren-6-yl)-acetamide

Guidance literature:: With hydrazine hydrate; In ethanol; for 3h; Heating;
DOI:10.1016/0223-5234(90)90194-8

Reference yield:

: 56872-55-0
2'-hydroxy-5'-acetamido-3-benzoyl-propionic acid

: 133414-49-0
N-(2-Oxo-2,3,10,10a-tetrahydro-1H-9-oxa-3,4-diaza-phenanthren-6-yl)-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 35 percent / 0.5 N NaOH / 1 h / 50 °C

2: 75 percent / hydrazine hydrate / ethanol / 3 h / Heating

With sodium hydroxide; hydrazine hydrate; In ethanol;
DOI:10.1016/0223-5234(90)90194-8

Reference yield:

: 51-66-1
4-methoxyacetanilide

: 133414-49-0
N-(2-Oxo-2,3,10,10a-tetrahydro-1H-9-oxa-3,4-diaza-phenanthren-6-yl)-acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / AlCl₃ / dimethylformamide / 1 h / 70 °C

2: 35 percent / 0.5 N NaOH / 1 h / 50 °C

3: 75 percent / hydrazine hydrate / ethanol / 3 h / Heating

With sodium hydroxide; aluminium trichloride; hydrazine hydrate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/0223-5234(90)90194-8