Technology Process of 1,3-bis-(4-allyl-2,6-diisopropylphenyl)imidazolium chloride
There total 4 articles about 1,3-bis-(4-allyl-2,6-diisopropylphenyl)imidazolium chloride which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
water;
In
tetrahydrofuran;
at 40 ℃;
for 16h;
Schlenk technique;
Glovebox;
Inert atmosphere;
DOI:10.1039/c4gc00642a
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 5,5-dimethyl-1,3-cyclohexadiene / 12 h / 120 °C / Schlenk technique; Glovebox; Inert atmosphere
2: zinc(II) chloride / 5,5-dimethyl-1,3-cyclohexadiene / 4 h / Reflux; Schlenk technique; Glovebox; Inert atmosphere
3: formic acid / isopropyl alcohol; water / Schlenk technique; Glovebox; Inert atmosphere
4: water / tetrahydrofuran / 16 h / 40 °C / Schlenk technique; Glovebox; Inert atmosphere
With
formic acid; water; zinc(II) chloride;
In
tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene; water; isopropyl alcohol;
2: |Aza-Claisen Rearrangement;
DOI:10.1039/c4gc00642a
- Guidance literature:
-
Multi-step reaction with 3 steps
1: zinc(II) chloride / 5,5-dimethyl-1,3-cyclohexadiene / 4 h / Reflux; Schlenk technique; Glovebox; Inert atmosphere
2: formic acid / isopropyl alcohol; water / Schlenk technique; Glovebox; Inert atmosphere
3: water / tetrahydrofuran / 16 h / 40 °C / Schlenk technique; Glovebox; Inert atmosphere
With
formic acid; water; zinc(II) chloride;
In
tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene; water; isopropyl alcohol;
1: |Aza-Claisen Rearrangement;
DOI:10.1039/c4gc00642a
