(S)-2,3-Dimethyl-1-(4-nitro-phenylsulfanyl)-but-3-en-2-yl-hydroperoxide

Base Information

Chemical Name:(S)-2,3-Dimethyl-1-(4-nitro-phenylsulfanyl)-but-3-en-2-yl-hydroperoxide
CAS No.:114597-60-3
Molecular Formula:C₁₂H₁₅NO₄S
Molecular Weight:269.321
Hs Code.:

Synonyms:(S)-2,3-Dimethyl-1-(4-nitro-phenylsulfanyl)-but-3-en-2-yl-hydroperoxide

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Chemical Property of (S)-2,3-Dimethyl-1-(4-nitro-phenylsulfanyl)-but-3-en-2-yl-hydroperoxide

Chemical Property:

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Technology Process of (S)-2,3-Dimethyl-1-(4-nitro-phenylsulfanyl)-but-3-en-2-yl-hydroperoxide

There total 3 articles about (S)-2,3-Dimethyl-1-(4-nitro-phenylsulfanyl)-but-3-en-2-yl-hydroperoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5072-70-8
1-bromo-2,3-dimethyl-2-butene

: 114597-60-3
(S)-2,3-Dimethyl-1-(4-nitro-phenylsulfanyl)-but-3-en-2-yl-hydroperoxide

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / sodium methoxide / ethanol / 1 h / Ambient temperature

2: O₂, Rose Bengal / acetone-d6 / -78 °C / Irradiation

With oxygen; sodium methylate; rose bengal; In ethanol; acetone;
DOI:10.1021/ja00203a023

Reference yield:

: 114597-58-9
1-[(4-nitrophenyl)thio]-2,3-dimethyl-2-butene

: 114597-60-3
(S)-2,3-Dimethyl-1-(4-nitro-phenylsulfanyl)-but-3-en-2-yl-hydroperoxide

: 114597-59-0
2-Methyl-3-(4-nitro-phenylsulfanylmethyl)-but-3-en-2-yl-hydroperoxide

Guidance literature:: With oxygen; rose bengal; In acetone; at -78 ℃; Irradiation;
DOI:10.1021/ja00203a023

Reference yield:

: 1849-36-1
para-nitrobenzenethiol

: 114597-60-3
(S)-2,3-Dimethyl-1-(4-nitro-phenylsulfanyl)-but-3-en-2-yl-hydroperoxide

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / sodium methoxide / ethanol / 1 h / Ambient temperature

2: O₂, Rose Bengal / acetone-d6 / -78 °C / Irradiation

With oxygen; sodium methylate; rose bengal; In ethanol; acetone;
DOI:10.1021/ja00203a023