2,6-Di-tert-butyl-4-(1,3-dithiolan-2-yliden)-2,5-cyclohexadien-1-on-S-oxid

Base Information

• Chemical Name: 2,6-Di-tert-butyl-4-(1,3-dithiolan-2-yliden)-2,5-cyclohexadien-1-on-S-oxid
• CAS No.: 113354-23-7
• Molecular Formula: C₁₇H₂₄O₂S₂
• Molecular Weight: 324.508

Synonyms:2,6-Di-tert-butyl-4-(1,3-dithiolan-2-yliden)-2,5-cyclohexadien-1-on-S-oxid

Chemical Property of 2,6-Di-tert-butyl-4-(1,3-dithiolan-2-yliden)-2,5-cyclohexadien-1-on-S-oxid

Chemical Property:

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Technology Process of 2,6-Di-tert-butyl-4-(1,3-dithiolan-2-yliden)-2,5-cyclohexadien-1-on-S-oxid

There total 1 articles about 2,6-Di-tert-butyl-4-(1,3-dithiolan-2-yliden)-2,5-cyclohexadien-1-on-S-oxid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

2,6-di-tert-butyl-4-[1,3]dithiolan-2-ylidene-cyclohexa-2,5-dienone (3152-80-5) → 2,6-Di-tert-butyl-4-(1,3-dithiolan-2-yliden)-2,5-cyclohexadien-1-on-S-oxid (113354-23-7)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid;

Reference yield: 96.0%

2,6-Di-tert-butyl-4-(1,3-dithiolan-2-yliden)-2,5-cyclohexadien-1-on-S-oxid (113354-23-7) → 2,6-di-tert-butyl-4-([1,3]dithiol-2-ylidene)cyclohexa-2,5-dienone (109857-96-7)

Guidance literature:

With trimethylsilyl iodide; N-ethyl-N,N-diisopropylamine; In dichloromethane; at -78 ℃; for 3h;

DOI:10.1055/s-1990-26849

Reference yield: 45.0%

2,6-Di-tert-butyl-4-(1,3-dithiolan-2-yliden)-2,5-cyclohexadien-1-on-S-oxid (113354-23-7) → 2,6-Di-tert-butyl-4-(1,3-dithiolan-2-yliden)-2,5-cyclohexadien-1-on-S,S-dioxid (113378-73-7)

Guidance literature:

With potassium permanganate; magnesium sulfate; In dichloromethane; water; for 0.5h; Ambient temperature;

upstream raw materials:

2,6-di-tert-butyl-4-[1,3]dithiolan-2-ylidene-cyclohexa-2,5-dienone

Downstream raw materials:

2,6-di-tert-butyl-4-([1,3]dithiol-2-ylidene)cyclohexa-2,5-dienone

2,6-Di-tert-butyl-4-(1,3-dithiolan-2-yliden)-2,5-cyclohexadien-1-on-S,S-dioxid

N,N-Dimethyl-4-hydroxy-3,5-di-tert.-butyl-thiobenzamid

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