(η5-pentamethylcyclopentadienyl)(η6-boratabenzene-Me-C3(CH3)3CHCCH2Ph)ruthenium

Base Information

• Chemical Name: (η5-pentamethylcyclopentadienyl)(η6-boratabenzene-Me-C3(CH3)3CHCCH2Ph)ruthenium
• CAS No.: 848469-35-2
• Molecular Formula: C₂₆H₃₅BRu
• Molecular Weight: 459.445

Synonyms:(η5-pentamethylcyclopentadienyl)(η6-boratabenzene-Me-C3(CH3)3CHCCH2Ph)ruthenium

Chemical Property of (η5-pentamethylcyclopentadienyl)(η6-boratabenzene-Me-C3(CH3)3CHCCH2Ph)ruthenium

Chemical Property:

Purity/Quality:

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Technology Process of (η5-pentamethylcyclopentadienyl)(η6-boratabenzene-Me-C3(CH3)3CHCCH2Ph)ruthenium

There total 1 articles about (η5-pentamethylcyclopentadienyl)(η6-boratabenzene-Me-C3(CH3)3CHCCH2Ph)ruthenium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

(η(5)-pentamethyl-2,3-dihydro-1,3-diborolyl)(η(5)-pentamethylcyclopentadienyl)ruthenium + propargyl benzene (10147-11-2) → (η5-pentamethylcyclopentadienyl)(η6-boratabenzene-Me-C3(CH3)3CHCCH2Ph)ruthenium (848469-35-2) + (η5-pentamethylcyclopentadienyl)(η7-4-borataborepine-Me2-C3(CH3)3CHCCH2Ph)ruthenium (848469-36-3)

Guidance literature:

In hexane; byproducts: tribenzylbenzene; 3-phenyl-1-propyne in hexane added to soln. of Ru complex in hexane at -45°C for 30 min, warmed to room temp.; filtered, filtrate evapd. to dryness under vac., recrystd. from CH2Cl2 at room temp.;

DOI:10.1002/anie.200461719

upstream raw materials:

propargyl benzene

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