N-[2-(benzo[1,3]dioxol-5-yl)ethyl]-2-(2,2-dichlorovinyl)-5,6-dimethoxybenzamide

Base Information

Chemical Name:N-[2-(benzo[1,3]dioxol-5-yl)ethyl]-2-(2,2-dichlorovinyl)-5,6-dimethoxybenzamide
CAS No.:550358-41-3
Molecular Formula:C₂₀H₁₉Cl₂NO₅
Molecular Weight:424.281
Hs Code.:

Synonyms:N-[2-(benzo[1,3]dioxol-5-yl)ethyl]-2-(2,2-dichlorovinyl)-5,6-dimethoxybenzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[2-(benzo[1,3]dioxol-5-yl)ethyl]-2-(2,2-dichlorovinyl)-5,6-dimethoxybenzamide

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Technology Process of N-[2-(benzo[1,3]dioxol-5-yl)ethyl]-2-(2,2-dichlorovinyl)-5,6-dimethoxybenzamide

There total 3 articles about N-[2-(benzo[1,3]dioxol-5-yl)ethyl]-2-(2,2-dichlorovinyl)-5,6-dimethoxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1484-85-1
3,4-methylenedioxyphenylethylamine

: 171779-77-4
2-(2,2-dichlorovinyl)-5,6-dimethoxybenzoic acid

: 550358-41-3
N-[2-(benzo[1,3]dioxol-5-yl)ethyl]-2-(2,2-dichlorovinyl)-5,6-dimethoxybenzamide

Guidance literature:: With diethyl cyanophosphonate; triethylamine; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.3987/com-02-s50

Reference yield:

: 550358-40-2
benzyl N-[2-(benzo[1,3]dioxol-5-yl)ethyl]carbamate

: 550358-41-3
N-[2-(benzo[1,3]dioxol-5-yl)ethyl]-2-(2,2-dichlorovinyl)-5,6-dimethoxybenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / H₂ / 5 percent Pd-C / methanol; tetrahydrofuran / 3 h / 20 °C / 760 Torr

2: 78 percent / diethyl phosphorocyanidate; Et₃N / tetrahydrofuran / 2 h / 20 °C

With diethyl cyanophosphonate; hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol;
DOI:10.3987/com-02-s50

Reference yield:

: 82735-27-1
6,7-dimethoxy-3-trichloromethyl-phthalide

: 550358-41-3
N-[2-(benzo[1,3]dioxol-5-yl)ethyl]-2-(2,2-dichlorovinyl)-5,6-dimethoxybenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / Zn powder / acetic acid; tetrahydrofuran / 4 h / 55 - 65 °C

2: 78 percent / diethyl phosphorocyanidate; Et₃N / tetrahydrofuran / 2 h / 20 °C

With diethyl cyanophosphonate; triethylamine; zinc; In tetrahydrofuran; acetic acid;
DOI:10.3987/com-02-s50