1,10-phenanthroline(4,7)-phenyl(4'):(1-oxa-3-(phenyl-3'',5''-diyl)propyl(3'',5''))G₁,G₂/2x,4x:(1-xa-4-oxa-7-oxa-10-oxaundecane)8-cascadane

Base Information

• Chemical Name: 1,10-phenanthroline(4,7)-phenyl(4'):(1-oxa-3-(phenyl-3'',5''-diyl)propyl(3'',5''))G₁,G₂/2x,4x:(1-xa-4-oxa-7-oxa-10-oxaundecane)8-cascadane
• CAS No.: 1095272-25-5
• Molecular Formula: C₁₂₂H₁₆₄N₂O₃₈
• Molecular Weight: 2266.63

Synonyms:1,10-phenanthroline(4,7)-phenyl(4'):(1-oxa-3-(phenyl-3'',5''-diyl)propyl(3'',5''))G₁,G₂/2x,4x:(1-xa-4-oxa-7-oxa-10-oxaundecane)8-cascadane

Chemical Property of 1,10-phenanthroline(4,7)-phenyl(4'):(1-oxa-3-(phenyl-3'',5''-diyl)propyl(3'',5''))G₁,G₂/2x,4x:(1-xa-4-oxa-7-oxa-10-oxaundecane)8-cascadane

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Technology Process of 1,10-phenanthroline(4,7)-phenyl(4'):(1-oxa-3-(phenyl-3'',5''-diyl)propyl(3'',5''))G₁,G₂/2x,4x:(1-xa-4-oxa-7-oxa-10-oxaundecane)8-cascadane

There total 1 articles about 1,10-phenanthroline(4,7)-phenyl(4'):(1-oxa-3-(phenyl-3'',5''-diyl)propyl(3'',5''))G₁,G₂/2x,4x:(1-xa-4-oxa-7-oxa-10-oxaundecane)8-cascadane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

4,7-bis(4'-hydroxyphenyl)-1,10-phenanthroline (900803-81-8) + 3,5-di-(3',5'-di-[1'',4'',7'',10''-tetraoxaundecyl]benzyloxy)benzyl bromide (288850-04-4) → 1,10-phenanthroline(4,7)-phenyl(4'):(1-oxa-3-(phenyl-3'',5''-diyl)propyl(3'',5''))G1,G2/2x,4x:(1-xa-4-oxa-7-oxa-10-oxaundecane)8-cascadane (1095272-25-5)

Guidance literature:

4,7-bis(4'-hydroxyphenyl)-1,10-phenanthroline; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; for 0.0833333h;

3,5-di-(3',5'-di-[1'',4'',7'',10''-tetraoxaundecyl]benzyloxy)benzyl bromide; In N,N-dimethyl-formamide; at 20 ℃; for 24h;

DOI:10.1039/b805136d

Reference yield:

1,10-phenanthroline(4,7)-phenyl(4'):(1-oxa-3-(phenyl-3'',5''-diyl)propyl(3'',5''))G1,G2/2x,4x:(1-xa-4-oxa-7-oxa-10-oxaundecane)8-cascadane (1095272-25-5) + water (7732-18-5) + copper(II) nitrate → diaquabis(1,10-phenanthroline(4,7)-phenyl(4'):(1-oxa-3-(phenyl-3'',5''-diyl)propyl(3'',5''))G1,G2/2x,4x:(1-oxa-4-oxa-7-oxa-10-oxaundecane)8-cascadane)copper(II)(2+)

Guidance literature:

In water; aq. soln. of ligand (2 equiv.) added to aq. soln. of Cu(NO3)2 at 20°C; not isolated; monitored by UV-vis, ESR and fluorescence spectra;

DOI:10.1039/b805136d

Reference yield:

copper-64 chloride + 1,10-phenanthroline(4,7)-phenyl(4'):(1-oxa-3-(phenyl-3'',5''-diyl)propyl(3'',5''))G1,G2/2x,4x:(1-xa-4-oxa-7-oxa-10-oxaundecane)8-cascadane (1095272-25-5) + water (7732-18-5) → diaquabis(1,10-phenanthroline(4,7)-phenyl(4'):(1-oxa-3-(phenyl-3'',5''-diyl)propyl(3'',5''))G1,G2/2x,4x:(1-oxa-4-oxa-7-oxa-10-oxaundecane)8-cascadane)copper-64(II)(2+)

Guidance literature:

With 2-(N-morpholino)ethanesulfonic acid; NaOH; In water; (64)CuCl in 2-(N-morpholino)ethanesulfonic acid-NaOH buffer added at room temp. to soln. of ligand in the same buffer, pH 5.4-7.4; not isolated; monitored by thin layer chromy.;

DOI:10.1039/b805136d

upstream raw materials:

4,7-bis(4'-hydroxyphenyl)-1,10-phenanthroline

3,5-di-(3',5'-di-[1'',4'',7'',10''-tetraoxaundecyl]benzyloxy)benzyl bromide

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