8-methoxycarbonyloctyl 3-O-(2-azido-2-deoxy-α-D-galactopyranosyl)-2,4-di-O-benzoyl-α-L-rhamnopyranoside

Base Information

Chemical Name:8-methoxycarbonyloctyl 3-O-(2-azido-2-deoxy-α-D-galactopyranosyl)-2,4-di-O-benzoyl-α-L-rhamnopyranoside
CAS No.:79264-13-4
Molecular Formula:C₃₆H₄₇N₃O₁₃
Molecular Weight:729.781
Hs Code.:

Synonyms:8-methoxycarbonyloctyl 3-O-(2-azido-2-deoxy-α-D-galactopyranosyl)-2,4-di-O-benzoyl-α-L-rhamnopyranoside

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Chemical Property of 8-methoxycarbonyloctyl 3-O-(2-azido-2-deoxy-α-D-galactopyranosyl)-2,4-di-O-benzoyl-α-L-rhamnopyranoside

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Technology Process of 8-methoxycarbonyloctyl 3-O-(2-azido-2-deoxy-α-D-galactopyranosyl)-2,4-di-O-benzoyl-α-L-rhamnopyranoside

There total 3 articles about 8-methoxycarbonyloctyl 3-O-(2-azido-2-deoxy-α-D-galactopyranosyl)-2,4-di-O-benzoyl-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 79264-10-1
8-methoxycarbonyloctyl 3-O-(3,4,6-tri-O-acetyl-2-azido-2-deoxy-α-D-galactopyranosyl)-2,4-di-O-benzoyl-α-L-rhamnopyranoside

: 79264-13-4
8-methoxycarbonyloctyl 3-O-(2-azido-2-deoxy-α-D-galactopyranosyl)-2,4-di-O-benzoyl-α-L-rhamnopyranoside

Guidance literature:: With magnesium methanolate; In methanol; at 0 ℃; for 16h;
DOI:10.1039/P19810002379

Reference yield:

: 67817-37-2
3,4,6-tri-O-acetyl-2-azido-2-deoxy-β-D-galactopyranosyl chloride

: 79264-13-4
8-methoxycarbonyloctyl 3-O-(2-azido-2-deoxy-α-D-galactopyranosyl)-2,4-di-O-benzoyl-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / silver trifluoromethanesulphonate, silver carbonate / CH₂Cl₂ / 4 h

2: 88 percent / magnesium methoxide / methanol / 16 h / 0 °C

With silver trifluoromethanesulfonate; magnesium methanolate; silver carbonate; In methanol; dichloromethane;
DOI:10.1039/P19810002379

Reference yield:

: 74597-41-4
8-(methoxycarbonyl)-octyl 2,4-di-O-benzoyl-α-L-rhamnopyranoside

: 79264-13-4
8-methoxycarbonyloctyl 3-O-(2-azido-2-deoxy-α-D-galactopyranosyl)-2,4-di-O-benzoyl-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / silver trifluoromethanesulphonate, silver carbonate / CH₂Cl₂ / 4 h

2: 88 percent / magnesium methoxide / methanol / 16 h / 0 °C

With silver trifluoromethanesulfonate; magnesium methanolate; silver carbonate; In methanol; dichloromethane;
DOI:10.1039/P19810002379