N-<2-(methoxycarbonyl)ethyl>-N-(9-phenylfluorenyl)-3-cyanoalanine benzyl ester

Base Information

Chemical Name:N-<2-(methoxycarbonyl)ethyl>-N-(9-phenylfluorenyl)-3-cyanoalanine benzyl ester
CAS No.:95407-38-8
Molecular Formula:C₃₄H₃₀N₂O₄
Molecular Weight:530.623
Hs Code.:

Synonyms:N-<2-(methoxycarbonyl)ethyl>-N-(9-phenylfluorenyl)-3-cyanoalanine benzyl ester

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Chemical Property of N-<2-(methoxycarbonyl)ethyl>-N-(9-phenylfluorenyl)-3-cyanoalanine benzyl ester

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Technology Process of N-<2-(methoxycarbonyl)ethyl>-N-(9-phenylfluorenyl)-3-cyanoalanine benzyl ester

There total 5 articles about N-<2-(methoxycarbonyl)ethyl>-N-(9-phenylfluorenyl)-3-cyanoalanine benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 55135-66-5
9-bromo-9-phenyl-9H-fluorene

: 95407-37-7
N-<2-(methoxycarbonyl)ethyl>-3-cyanoalanine benzyl ester

: 95407-38-8
N-<2-(methoxycarbonyl)ethyl>-N-(9-phenylfluorenyl)-3-cyanoalanine benzyl ester

Guidance literature:: With potassium phosphate; lead(II) nitrate; In acetonitrile; for 4h;
DOI:10.1021/jo00208a017

Reference yield:

: 95407-34-4
N-(2-(methoxycarbonyl)ethyl)asparagine

: 95407-38-8
N-<2-(methoxycarbonyl)ethyl>-N-(9-phenylfluorenyl)-3-cyanoalanine benzyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 50 percent / Et₃N / H₂O; propan-1-ol / 24 h

2: Et₃N / tetrahydrofuran / 2 h / Heating

3: TsCl, pyridine / CH₂Cl₂ / 24 h

4: water, TFA / acetonitrile / 1 h

5: 88 percent / K₃PO₄, Pb(NO₃)2 / acetonitrile / 4 h

With pyridine; potassium phosphate; lead(II) nitrate; water; triethylamine; p-toluenesulfonyl chloride; trifluoroacetic acid; In tetrahydrofuran; propan-1-ol; dichloromethane; water; acetonitrile;
DOI:10.1021/jo00208a017

Reference yield:

: 95407-35-5
N-<(tert-butyloxy)carbonyl>-N-<2-(methoxycarbonyl)ethyl>asparagine

: 95407-38-8
N-<2-(methoxycarbonyl)ethyl>-N-(9-phenylfluorenyl)-3-cyanoalanine benzyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: Et₃N / tetrahydrofuran / 2 h / Heating

2: TsCl, pyridine / CH₂Cl₂ / 24 h

3: water, TFA / acetonitrile / 1 h

4: 88 percent / K₃PO₄, Pb(NO₃)2 / acetonitrile / 4 h

With pyridine; potassium phosphate; lead(II) nitrate; water; triethylamine; p-toluenesulfonyl chloride; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/jo00208a017