{(n-C₄H₉)4N}{BBr₄}

Base Information

Chemical Name:{(n-C₄H₉)4N}{BBr₄}
CAS No.:61132-54-5
Molecular Formula:BBr₄*C₁₆H₃₆N
Molecular Weight:572.896
Hs Code.:

{(n-C<sub>4</sub>H<sub>9</sub>)4N}{BBr<sub>4</sub>}

Synonyms:{(n-C₄H₉)4N}{BBr₄}

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Chemical Property of {(n-C₄H₉)4N}{BBr₄}

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Technology Process of {(n-C₄H₉)4N}{BBr₄}

There total 8 articles about {(n-C₄H₉)4N}{BBr₄} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: [dicarbonyl(π-cyclopentadienyl)(4-trifluoromethylphenylcarbene)manganese]BBr4

: 1643-19-2
tetrabutylammomium bromide

: 61132-54-5
{(n-C₄H₉)4N}{BBr₄}

: [dicarbonyl(π-cyclopentadienyl)(bromo(4-trifluoromethylphenyl)carbene)manganese]

Guidance literature:: In further solvent(s); under N2, to CH3I soln. of Mn complex at -78°C added with stirring (C4H9)4NBr by portions, warmed to -50°C, stirred for 0.5 h; solvent removed in vac., chromd. on Al2O3 at -80°C with CH3I/pentane or extracted with CH3I/pentane (1/10), recrystd. from this solventsmixt., elem. anal.;
DOI:10.1016/0022-328X(83)80121-1

Reference yield: 49.0%

: [dicarbonyl(π-cyclopentadienyl)(4-trifluoromethylphenylcarbene)rhenium]BBr4

: 1112-67-0
tetrabutyl-ammonium chloride

: 61132-54-5
{(n-C₄H₉)4N}{BBr₄}

: [dicarbonyl(π-cyclopentadienyl)(bromo(4-trifluoromethylphenyl)carbene)rhenium]

Guidance literature:: In further solvent(s); under N2, to CH3I soln. of Re complex added by portions at -80°Cwith stirring (C4H9)4NBr, warmed at -45°C, stirred for 0.5 h at this temp.; added cooled pentane, filtered, filtrate evapd. at -45°C to dryness, residue extracted with pentane at -40°C, extract cooled to -78°C, elem. anal.;
DOI:10.1016/0022-328X(83)80121-1

Reference yield: 46.0%

: [dicarbonyl(π-cyclopentadienyl)(4-trifluoromethylphenylcarbene)rhenium]BBr4

: 311-28-4
tetra-(n-butyl)ammonium iodide

: 61132-54-5
{(n-C₄H₉)4N}{BBr₄}

: [dicarbonyl(π-cyclopentadienyl)(iodo(4-trifluoromethylphenyl)carbene)rhenium]

Guidance literature:: In further solvent(s); under N2, to CH3I soln. of Re complex added by portions at -80°Cwith stirring (C4H9)4NI, warmed to -40°C, stirred for 2-3 h at this temp.; added cooled pentane, filtered, filtrate evapd. at -45°C to dryness, residue extracted with pentane at -40°C, extract cooled to -78°C, elem. anal.;
DOI:10.1016/0022-328X(83)80121-1