3-(2-Chloroethoxy)-5-(prop-2-enoxymethyl)aniline

Base Information

Chemical Name:3-(2-Chloroethoxy)-5-(prop-2-enoxymethyl)aniline
CAS No.:1312603-47-6
Molecular Formula:C₁₂H₁₆ClNO₂
Molecular Weight:241.718
Hs Code.:
DSSTox Substance ID:DTXSID001193880

Synonyms:1312603-47-6;DTXSID001193880;3-(2-Chloroethoxy)-5-[(2-propen-1-yloxy)methyl]benzenamine

Suppliers and Price of 3-(2-Chloroethoxy)-5-(prop-2-enoxymethyl)aniline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(2-Chloroethoxy)-5-(prop-2-enoxymethyl)aniline

Chemical Property:

XLogP3:2.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:7
Exact Mass:241.0869564
Heavy Atom Count:16
Complexity:202

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C=CCOCC1=CC(=CC(=C1)OCCCl)N

Technology Process of 3-(2-Chloroethoxy)-5-(prop-2-enoxymethyl)aniline

There total 4 articles about 3-(2-Chloroethoxy)-5-(prop-2-enoxymethyl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1312603-40-9
1-allyloxymethyl-3-(2-chloroethoxy)-5-nitrobenzene

: 1312603-47-6
5-(2-chloroethoxy)-3-[(prop-2-en-1-yloxy)methyl]aniline

Guidance literature:: With iron; ammonium chloride; In ethanol; water; at 50 - 80 ℃; for 4h;
DOI:10.1021/jm200326p

Reference yield:

: 1312603-33-0
3-(2-chloro-ethoxy)-5-nitrobenzaldehyde

: 1312603-47-6
5-(2-chloroethoxy)-3-[(prop-2-en-1-yloxy)methyl]aniline

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tetrahydroborate / tetrahydrofuran / 0 - 20 °C

2: tetra(n-butyl)ammonium hydrogensulfate; potassium hydroxide / 12 h / 20 °C

3: iron; ammonium chloride / ethanol; water / 4 h / 50 - 80 °C

With sodium tetrahydroborate; tetra(n-butyl)ammonium hydrogensulfate; iron; ammonium chloride; potassium hydroxide; In tetrahydrofuran; ethanol; water;
DOI:10.1021/jm200326p

Reference yield:

: 1312603-35-2
[3-(2-chloroethoxy)-5-nitrophenyl]methanol

: 1312603-47-6
5-(2-chloroethoxy)-3-[(prop-2-en-1-yloxy)methyl]aniline

Guidance literature:: Multi-step reaction with 2 steps

1: tetra(n-butyl)ammonium hydrogensulfate; potassium hydroxide / 12 h / 20 °C

2: iron; ammonium chloride / ethanol; water / 4 h / 50 - 80 °C

With tetra(n-butyl)ammonium hydrogensulfate; iron; ammonium chloride; potassium hydroxide; In ethanol; water;
DOI:10.1021/jm200326p