Technology Process of C30H31F4N3O5S
There total 11 articles about C30H31F4N3O5S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium fluoride; tetrakis(triphenylphosphine) palladium(0);
In
1,2-dimethoxyethane; water;
at 90 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: lithium hydroxide; water / tetrahydrofuran / 2 h / 0 - 20 °C
1.2: pH 5
2.1: triethylamine / dichloromethane / 3 h / 0 - 20 °C
3.1: ammonium acetate / toluene / 5 h / 110 °C
4.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate / 1,2-dimethoxyethane / 2 h / 90 °C / Inert atmosphere
5.1: tetrakis(triphenylphosphine) palladium(0); potassium fluoride / 1,2-dimethoxyethane; water / 2 h / 90 °C
With
potassium fluoride; tetrakis(triphenylphosphine) palladium(0); dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; ammonium acetate; water; potassium acetate; triethylamine; lithium hydroxide;
In
tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; water; toluene;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: diethylamino-sulfur trifluoride / dichloromethane / 21 h / -78 - 20 °C
2.1: lithium hydroxide; water / tetrahydrofuran / 2 h / 0 - 20 °C
2.2: pH 5
3.1: triethylamine / dichloromethane / 3 h / 0 - 20 °C
4.1: ammonium acetate / toluene / 5 h / 110 °C
5.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate / 1,2-dimethoxyethane / 2 h / 90 °C / Inert atmosphere
6.1: tetrakis(triphenylphosphine) palladium(0); potassium fluoride / 1,2-dimethoxyethane; water / 2 h / 90 °C
With
potassium fluoride; tetrakis(triphenylphosphine) palladium(0); dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; diethylamino-sulfur trifluoride; ammonium acetate; water; potassium acetate; triethylamine; lithium hydroxide;
In
tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; water; toluene;