tris(perfluorophenyl)borane-acetonitrile adduct

Base Information

• Chemical Name: tris(perfluorophenyl)borane-acetonitrile adduct
• CAS No.: 212619-93-7
• Molecular Formula: C₂₀H₃BF₁₅N
• Molecular Weight: 553.038
• Mol file: 212619-93-7.mol

Synonyms:tris(perfluorophenyl)borane-acetonitrile adduct

Chemical Property of tris(perfluorophenyl)borane-acetonitrile adduct

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tris(perfluorophenyl)borane-acetonitrile adduct

There total 14 articles about tris(perfluorophenyl)borane-acetonitrile adduct which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

tris(pentafluorophenyl)borate (1109-15-5) + acetonitrile (75-05-8,26809-02-9) → tris(perfluorophenyl)borane-acetonitrile adduct (212619-93-7)

Guidance literature:

Inert atmosphere; Sealed tube;

DOI:10.1002/zaac.202000030

Reference yield:

[(Me4C5NH)CO2B(C6F5)3] + acetonitrile (75-05-8,26809-02-9) → 2,2,6,6-tetramethyl-piperidine (768-66-1) + tris(perfluorophenyl)borane-acetonitrile adduct (212619-93-7)

Guidance literature:

In dichloromethane-d2; Inert atmosphere; Glovebox;

DOI:10.1039/c5dt03008k

Reference yield:

C22H13BF12O (1416345-15-7) → tris(perfluorophenyl)borane-acetonitrile adduct (212619-93-7)

Guidance literature:

Multi-step reaction with 3 steps

1: dimethylmonochlorosilane / hexane / 3 h / Inert atmosphere

2: dichloromethane-d2 / Inert atmosphere

3: dichloromethane-d2 / Inert atmosphere

With dimethylmonochlorosilane; In hexane; dichloromethane-d2;

DOI:10.1021/om3011195

upstream raw materials:

tris(pentafluorophenyl)borate

acetonitrile

tris(β-perfluoronaphthyl)borane-acetonitrile adduct

(CH₂CHCH₂)Ni(NCCH₃)2⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=(CH₂CHCH₂)Ni(NCCH₃)2B(C₆H₃(CF₃)2)4

Downstream raw materials:

C₆F₄B₂(C₆F₅)2C₆F₄CH₃CN

tris(pentafluorophenyl)borate

tris(β-perfluoronaphthyl)borane-acetonitrile adduct

EtNH₂B(C₆F₅)3