rac-(E)-N-(2-methyl-1,3-diphenylprop-2-enyl)-(N,N-dimethylamino)sulfonamide

Base Information

• Chemical Name: rac-(E)-N-(2-methyl-1,3-diphenylprop-2-enyl)-(N,N-dimethylamino)sulfonamide
• CAS No.: 1239456-50-8
• Molecular Formula: C₁₈H₂₂N₂O₂S
• Molecular Weight: 330.451

Synonyms:rac-(E)-N-(2-methyl-1,3-diphenylprop-2-enyl)-(N,N-dimethylamino)sulfonamide

Chemical Property of rac-(E)-N-(2-methyl-1,3-diphenylprop-2-enyl)-(N,N-dimethylamino)sulfonamide

Chemical Property:

Purity/Quality:

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Technology Process of rac-(E)-N-(2-methyl-1,3-diphenylprop-2-enyl)-(N,N-dimethylamino)sulfonamide

There total 1 articles about rac-(E)-N-(2-methyl-1,3-diphenylprop-2-enyl)-(N,N-dimethylamino)sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

1-Phenylprop-1-yne (673-32-5) + N,N-Dimethyl-2-phenylethylensulfonamid (13719-45-4) → rac-(E)-N-(2-methyl-1,3-diphenylprop-2-enyl)-(N,N-dimethylamino)sulfonamide (1239456-50-8)

Guidance literature:

With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; tributylphosphine; diethylzinc; In 1,2-dimethoxyethane; toluene; at 25 ℃; for 2h; chemoselective reaction;

DOI:10.1021/ja104505t

Reference yield: 60.0%

rac-(E)-N-(2-methyl-1,3-diphenylprop-2-enyl)-(N,N-dimethylamino)sulfonamide (1239456-50-8) → C11H16N2O3S

Guidance literature:

With sodium periodate; ruthenium(III) chloride monohydrate; In tetrachloromethane; water; acetonitrile; for 24h;

DOI:10.1021/ja104505t

Reference yield:

rac-(E)-N-(2-methyl-1,3-diphenylprop-2-enyl)-(N,N-dimethylamino)sulfonamide (1239456-50-8) → (R)-(E)-2-methyl-1,3-diphenyl-2-propen-1-amine + (S)-(E)-2-methyl-1,3-diphenyl-2-propen-1-amine (1239456-95-1)

Guidance literature:

In Trimethylenediamine; for 2h; optical yield given as %ee; Reflux;

DOI:10.1021/ja104505t

upstream raw materials:

1-Phenylprop-1-yne

N,N-Dimethyl-2-phenylethylensulfonamid

Downstream raw materials:

(S)-(E)-2-methyl-1,3-diphenyl-2-propen-1-amine

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