4,4'-DIBROMO-4''-PHENYLTRIPHENYLAMINE

Base Information

• Chemical Name: 4,4'-DIBROMO-4''-PHENYLTRIPHENYLAMINE
• CAS No.: 884530-69-2
• Molecular Formula: C24H17Br2N
• Molecular Weight: 479.214
• Hs Code.: 29215900
• Mol file: 884530-69-2.mol

Synonyms:N,N-Bis(4-bromophenyl)biphenyl-4-amine;

Chemical Property of 4,4'-DIBROMO-4''-PHENYLTRIPHENYLAMINE

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Melting Point: 136.0 to 140.0 °C
• Refractive Index: 1.679
• Boiling Point: 573.643 °C at 760 mmHg
• PKA: -4.34±0.50(Predicted)
• Flash Point: 300.729 °C
• PSA: 3.24000
• Density: 1.506 g/cm³
• LogP: 8.34840
• Storage Temp.: Sealed in dry,Room Temperature
• Solubility.: soluble in Tetrahydrofuran

Purity/Quality:

99%, ^*data from raw suppliers

4,4''-Dibromo-4''''-phenyltriphenylamine ^*data from reagent suppliers

Safty Information:

• Safety Statements: 24/25

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4,4'-DIBROMO-4''-PHENYLTRIPHENYLAMINE

There total 1 articles about 4,4'-DIBROMO-4''-PHENYLTRIPHENYLAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

N,N-bis(phenyl)-4-biphenylamine (4432-94-4) → N,N-bis(4-bromophenyl)-[1,1’-biphenyl]-4-amine (884530-69-2)

Guidance literature:

With N-Bromosuccinimide; In ethyl acetate; toluene; for 27.5h;

Reference yield: 81.0%

N,N-bis(4-bromophenyl)-[1,1’-biphenyl]-4-amine (884530-69-2) + 6-phenylbenzo[b]naphtho[1,2-d]furan-8-boronic acid → 4,4'-bis(6-phenylbenzo[b]naphtho[1,2-d]furan-8-yl)-4-phenyltriphenylamine

Guidance literature:

With palladium diacetate; potassium carbonate; tris-(o-tolyl)phosphine; In ethanol; water; toluene; at 60 - 80 ℃; for 6.5h; Inert atmosphere;

Reference yield: 76.6%

N,N-bis(4-bromophenyl)-[1,1’-biphenyl]-4-amine (884530-69-2) + C11H8BNO3 → C46H29N3O2

Guidance literature:

With palladium diacetate; sodium carbonate; tris-(o-tolyl)phosphine; In water; for 15h; Reflux;

upstream raw materials:

N,N-bis(phenyl)-4-biphenylamine

Downstream raw materials:

4,4'-di-(1-naphthyl)-4-phenyltriphenylamine

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