3-benzyloxycarbonyl-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsaurenitril

Base Information

Chemical Name:3-benzyloxycarbonyl-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsaurenitril
CAS No.:114476-24-3
Molecular Formula:C₂₃H₂₃N₃O₂
Molecular Weight:373.455
Hs Code.:

Synonyms:3-benzyloxycarbonyl-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsaurenitril

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Chemical Property of 3-benzyloxycarbonyl-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsaurenitril

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Technology Process of 3-benzyloxycarbonyl-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsaurenitril

There total 9 articles about 3-benzyloxycarbonyl-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsaurenitril which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 143-33-9,25596-52-5
sodium cyanide

: 114476-23-2
3-benzyloxycarbonyl-7-acetoxy-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol

: 114476-24-3
3-benzyloxycarbonyl-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsaurenitril

Guidance literature:: With tetrabutylammomium bromide; sodium iodide; In toluene; for 3h; Heating;
DOI:10.1016/S0040-4020(01)86861-7

Reference yield: 44.0%

: 885-40-5
(+/-)-harmacine

: 143-33-9,25596-52-5
sodium cyanide

: 501-53-1,94274-21-2
benzyl chloroformate

: 114476-24-3
3-benzyloxycarbonyl-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsaurenitril

Guidance literature:: In tetrahydrofuran; acetone; for 1h; Ambient temperature; Heating;
DOI:10.1016/S0040-4020(01)86861-7

Reference yield:

: 114476-07-2
3-cyan-1,2,3,4,5,6,7,8-octahydoazonino<5,4-b>indol-7-carbonitril

: 114476-24-3
3-benzyloxycarbonyl-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsaurenitril

Guidance literature:: Multi-step reaction with 3 steps

1: 71 percent / potassium hydroxide / 0.42 h / Heating

2: 64 percent / 80 percent acetic acid / 60 h / Heating

3: 44 percent / tetrahydrofuran; acetone / 1 h / Ambient temperature; Heating

With potassium hydroxide; acetic acid; In tetrahydrofuran; acetone;
DOI:10.1016/S0040-4020(01)86861-7