1,3-bis(2,4,6-triisopropylbenzyl)(5,6-dimethyl)benzimidazolium bromide

Base Information

Chemical Name:1,3-bis(2,4,6-triisopropylbenzyl)(5,6-dimethyl)benzimidazolium bromide
CAS No.:1453079-66-7
Molecular Formula:Br*C₄₁H₅₉N₂
Molecular Weight:659.837
Hs Code.:

Synonyms:1,3-bis(2,4,6-triisopropylbenzyl)(5,6-dimethyl)benzimidazolium bromide

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Chemical Property of 1,3-bis(2,4,6-triisopropylbenzyl)(5,6-dimethyl)benzimidazolium bromide

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Technology Process of 1,3-bis(2,4,6-triisopropylbenzyl)(5,6-dimethyl)benzimidazolium bromide

There total 1 articles about 1,3-bis(2,4,6-triisopropylbenzyl)(5,6-dimethyl)benzimidazolium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 582-60-5
5,6-dimethyl-1H-benzo[d]imida-zole

: 166519-14-8
2-(bromomethyl)-1,3,5-triisopropylbenzene

: 1453079-66-7
1,3-bis(2,4,6-triisopropylbenzyl)(5,6-dimethyl)benzimidazolium bromide

Guidance literature:: 5,6-dimethyl-1H-benzo[d]imida-zole; With potassium carbonate; In acetonitrile; at 20 ℃; for 1h;

2-(bromomethyl)-1,3,5-triisopropylbenzene; In acetonitrile; for 24h; Reflux;

at 160 ℃; for 2h;
DOI:10.1021/ic401626e

Reference yield: 81.0%

: 12112-67-3
bis(1,5-cyclooctadiene)diiridium(I) dichloride

: 1453079-66-7
1,3-bis(2,4,6-triisopropylbenzyl)(5,6-dimethyl)benzimidazolium bromide

: chloro(η⁴-1,5-cyclooctadiene)[1,3-bis(2,4,6-triisopropylbenzyl)-5,6-dimethylbenzimidazol-2-ylidene]iridium(I)

Guidance literature:: 1,3-bis(2,4,6-triisopropylbenzyl)(5,6-dimethyl)benzimidazolium bromide; With silver(l) oxide; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere; Darkness;

bis(1,5-cyclooctadiene)diiridium(I) dichloride; In dichloromethane; at 20 ℃; for 12h; Inert atmosphere; Darkness;
DOI:10.1021/ic401626e