C₂₅H₄₂O₃

Base Information

Chemical Name:C₂₅H₄₂O₃
CAS No.:1310801-74-1
Molecular Formula:C₂₅H₄₂O₃
Molecular Weight:390.607
Hs Code.:

C<sub>25</sub>H<sub>42</sub>O<sub>3</sub>

Synonyms:C₂₅H₄₂O₃

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Chemical Property of C₂₅H₄₂O₃

Chemical Property:

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Technology Process of C₂₅H₄₂O₃

There total 15 articles about C₂₅H₄₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1310801-73-0
C₂₆H₄₄O₄S

: 1310801-74-1
C₂₅H₄₂O₃

Guidance literature:: With methanesulfonamide; AD-mix β; In water; tert-butyl alcohol; at 0 - 20 ℃; for 30h;
DOI:10.1016/j.tetlet.2011.03.089

Reference yield:

: 1310801-69-4
C₁₈H₂₈O₄

: 1310801-74-1
C₂₅H₄₂O₃

Guidance literature:: Multi-step reaction with 5 steps

1: n-butyllithium; methyl-triphenylphosphonium iodide / tetrahydrofuran / 0 - 20 °C

2: toluene-4-sulfonic acid / methanol / 0.5 h / Reflux

3: dmap; triethylamine / dichloromethane / 4 h / 0 - 20 °C

4: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 10 h / Reflux

5: AD-mix β; methanesulfonamide / water; tert-butyl alcohol / 30 h / 0 - 20 °C

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; dmap; n-butyllithium; methanesulfonamide; AD-mix β; methyl-triphenylphosphonium iodide; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water; tert-butyl alcohol; 1: Wittig reaction / 4: Cross methathesis / 5: Sharpless asymmetric dihydroxylation;
DOI:10.1016/j.tetlet.2011.03.089

Reference yield:

: 1310801-70-7
C₁₉H₃₀O₃

: 1310801-74-1
C₂₅H₄₂O₃

Guidance literature:: Multi-step reaction with 4 steps

1: toluene-4-sulfonic acid / methanol / 0.5 h / Reflux

2: dmap; triethylamine / dichloromethane / 4 h / 0 - 20 °C

3: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 10 h / Reflux

4: AD-mix β; methanesulfonamide / water; tert-butyl alcohol / 30 h / 0 - 20 °C

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; dmap; methanesulfonamide; AD-mix β; toluene-4-sulfonic acid; triethylamine; In methanol; dichloromethane; water; tert-butyl alcohol; 3: Cross methathesis / 4: Sharpless asymmetric dihydroxylation;
DOI:10.1016/j.tetlet.2011.03.089