methyl 4-(2-(5-chloro-2-octamethyleneimino-benzylamino)-ethyl)-2-methoxy-benzoate

Base Information

Chemical Name:methyl 4-(2-(5-chloro-2-octamethyleneimino-benzylamino)-ethyl)-2-methoxy-benzoate
CAS No.:219921-51-4
Molecular Formula:C₂₆H₃₃ClN₂O₄
Molecular Weight:473.012
Hs Code.:

Synonyms:methyl 4-(2-(5-chloro-2-octamethyleneimino-benzylamino)-ethyl)-2-methoxy-benzoate

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Chemical Property of methyl 4-(2-(5-chloro-2-octamethyleneimino-benzylamino)-ethyl)-2-methoxy-benzoate

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Technology Process of methyl 4-(2-(5-chloro-2-octamethyleneimino-benzylamino)-ethyl)-2-methoxy-benzoate

There total 5 articles about methyl 4-(2-(5-chloro-2-octamethyleneimino-benzylamino)-ethyl)-2-methoxy-benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 4-(2-amino-ethyl)-2-methoxy-benzoic acid methyl ester

: 78251-85-1
5-chloro-2-octamethyleneimino-benzoic acid

: 219921-51-4
methyl 4-(2-(5-chloro-2-octamethyleneimino-benzylamino)-ethyl)-2-methoxy-benzoate

Guidance literature:: With pyridine; at 100 ℃; for 48h;
DOI:10.1021/jm9810349

Reference yield:

: 5661-71-2
azonane

: 219921-51-4
methyl 4-(2-(5-chloro-2-octamethyleneimino-benzylamino)-ethyl)-2-methoxy-benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / Na₂CO₃ / ethanol / 4 h / Heating

2: 96 percent / H₂ / 10 percent Pd/C / methanol / 1 h / 20 °C / 3750.3 Torr

3: 1.) aq. NaNO₂, aq. HCl, 2.) Cu, aq. HCl / 1.) 0 deg C, 20 min, 2.) RT, 12 h

4: 46 percent / pyridine / 48 h / 100 °C

With pyridine; hydrogenchloride; hydrogen; copper; sodium carbonate; sodium nitrite; palladium on activated charcoal; In methanol; ethanol;
DOI:10.1021/jm9810349

Reference yield:

: 2516-96-3
2-chloro-5-nitrobenzoic acid

: 219921-51-4
methyl 4-(2-(5-chloro-2-octamethyleneimino-benzylamino)-ethyl)-2-methoxy-benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / Na₂CO₃ / ethanol / 4 h / Heating

2: 96 percent / H₂ / 10 percent Pd/C / methanol / 1 h / 20 °C / 3750.3 Torr

3: 1.) aq. NaNO₂, aq. HCl, 2.) Cu, aq. HCl / 1.) 0 deg C, 20 min, 2.) RT, 12 h

4: 46 percent / pyridine / 48 h / 100 °C

With pyridine; hydrogenchloride; hydrogen; copper; sodium carbonate; sodium nitrite; palladium on activated charcoal; In methanol; ethanol;
DOI:10.1021/jm9810349