benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside 4-(dibenzyl phosphate)

Base Information

Chemical Name:benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside 4-(dibenzyl phosphate)
CAS No.:122351-24-0
Molecular Formula:C₄₃H₄₆NO₉P
Molecular Weight:751.813
Hs Code.:

Synonyms:benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside 4-(dibenzyl phosphate)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside 4-(dibenzyl phosphate)

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Technology Process of benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside 4-(dibenzyl phosphate)

There total 5 articles about benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside 4-(dibenzyl phosphate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 62867-63-4
benzyl 2-acetamido-2-deoxy-3,6-di-O-benzyl-β-D-glucopyranoside

: 990-91-0
dibenzyl [[bis(benzyloxy)phosphoryl]oxy]phosphonate

: 122351-24-0
benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside 4-(dibenzyl phosphate)

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; hexane; at 0 ℃; for 1h;

Reference yield:

: 14855-31-3
benzyl 2-acetamido-3-O-benzyl-2-deoxy-β-D-glucopyranoside

: 122351-24-0
benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside 4-(dibenzyl phosphate)

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) bis(tributylstannyl)oxide, 2.) tetrabutylammonium iodide / 1.) toluene, reflux, 16 h, 2.) reflux, 4 h

2: 55 percent / lithium di-isopropylamide / tetrahydrofuran; hexane / 1 h / 0 °C

With tetra-(n-butyl)ammonium iodide; bis(tri-n-butyltin)oxide; lithium diisopropyl amide; In tetrahydrofuran; hexane;

Reference yield:

: 50605-13-5
benzyl 2-acetamido-3-O-benzyl-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranoside

: 122351-24-0
benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside 4-(dibenzyl phosphate)

Guidance literature:: Multi-step reaction with 3 steps

1: 80.65 percent / trifluoroacetic acid / methanol; H₂O

2: 1.) bis(tributylstannyl)oxide, 2.) tetrabutylammonium iodide / 1.) toluene, reflux, 16 h, 2.) reflux, 4 h

3: 55 percent / lithium di-isopropylamide / tetrahydrofuran; hexane / 1 h / 0 °C

With tetra-(n-butyl)ammonium iodide; trifluoroacetic acid; bis(tri-n-butyltin)oxide; lithium diisopropyl amide; In tetrahydrofuran; methanol; hexane; water;