cis-2,6-dibenzylpiperidine

Base Information

Chemical Name:cis-2,6-dibenzylpiperidine
CAS No.:1101197-07-2
Molecular Formula:C₁₉H₂₃N
Molecular Weight:265.398
Hs Code.:

Synonyms:cis-2,6-dibenzylpiperidine

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Chemical Property of cis-2,6-dibenzylpiperidine

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Technology Process of cis-2,6-dibenzylpiperidine

There total 5 articles about cis-2,6-dibenzylpiperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 11-benzyl-13-phenyl-7a,8,9,10,11,13-hexahydronaphtho[1,2-e]pyrido[2,1-b][1,3]oxazine

: 6921-34-2
benzylmagnesium chloride

: 1101197-07-2,5438-04-0
cis-2,6-dibenzylpiperidine

Guidance literature:: In tetrahydrofuran; at -3 - 20 ℃; for 12h; Inert atmosphere;
DOI:10.1039/c6ob02257j

Reference yield: 62.0%

: 47090-47-1
2,6-dibenzylpyridine

: 1101197-07-2,5438-04-0
cis-2,6-dibenzylpiperidine

Guidance literature:: With pyridine; H₂SiEt₂; tris(pentafluorophenyl)borate; hydrogen; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane; In toluene; at 100 ℃; under 30003 Torr; Autoclave;
DOI:10.1021/acscatal.1c02876

Reference yield:

: 13-phenyl-7a,8,9,10,11,13-hexahydronaphtho[1,2-e]pyrido[2,1-b][1,3]oxazine

: 1101197-07-2,5438-04-0
cis-2,6-dibenzylpiperidine

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran; diethyl ether / 2 h / -3 - 20 °C / Inert atmosphere

2: silver(l) oxide / m-xylene / 18 h / 140 °C

3: tetrahydrofuran / 12 h / -3 - 20 °C / Inert atmosphere

With silver(l) oxide; In tetrahydrofuran; diethyl ether; m-xylene;
DOI:10.1039/c6ob02257j