2-[tert-butoxycarbonylamino]-(2R,3S,4E)-5-(4-methoxyphenyl)-pent-4-en-3-ol

Base Information

Chemical Name:2-[tert-butoxycarbonylamino]-(2R,3S,4E)-5-(4-methoxyphenyl)-pent-4-en-3-ol
CAS No.:852310-56-6
Molecular Formula:C₁₇H₂₅NO₄
Molecular Weight:307.39
Hs Code.:

Synonyms:2-[tert-butoxycarbonylamino]-(2R,3S,4E)-5-(4-methoxyphenyl)-pent-4-en-3-ol

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Chemical Property of 2-[tert-butoxycarbonylamino]-(2R,3S,4E)-5-(4-methoxyphenyl)-pent-4-en-3-ol

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Technology Process of 2-[tert-butoxycarbonylamino]-(2R,3S,4E)-5-(4-methoxyphenyl)-pent-4-en-3-ol

There total 14 articles about 2-[tert-butoxycarbonylamino]-(2R,3S,4E)-5-(4-methoxyphenyl)-pent-4-en-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 852310-64-6
4-azido-1-(4-methoxyphenyl)-(E,3S,4R)-1-penten-3-ol

: 24424-99-5
di-tert-butyl dicarbonate

: 852310-56-6
2-[tert-butoxycarbonylamino]-(2R,3S,4E)-5-(4-methoxyphenyl)-pent-4-en-3-ol

Guidance literature:: 4-azido-1-(4-methoxyphenyl)-(E,3S,4R)-1-penten-3-ol; With triphenylphosphine; In water; benzene; at 45 ℃;

di-tert-butyl dicarbonate; With triethylamine;
DOI:10.1016/j.tetlet.2005.02.140

Reference yield: 85.0%

: 906478-62-4
2-[tert-butoxycarbonylamino]-(2R,3S,4E)-5-(4-methoxyphenyl)-pent-4-ene-1,3-diol

: 852310-56-6
2-[tert-butoxycarbonylamino]-(2R,3S,4E)-5-(4-methoxyphenyl)-pent-4-en-3-ol

: (R)-4-[(E)-(S)-1-Hydroxy-3-(4-methoxy-phenyl)-allyl]-oxazolidin-2-one

Guidance literature:: 2-[tert-butoxycarbonylamino]-(2R,3S,4E)-5-(4-methoxyphenyl)-pent-4-ene-1,3-diol; With di(n-butyl)tin oxide; triethylamine; p-toluenesulfonyl chloride; In dichloromethane; at 0 ℃;

With sodium tetrahydroborate; In dichloromethane; dimethyl sulfoxide; at 70 ℃;
DOI:10.1016/j.tetasy.2006.05.007

Reference yield: 83.0%

: 1258886-33-7
C₁₇H₂₃NO₄

: 852310-56-6
2-[tert-butoxycarbonylamino]-(2R,3S,4E)-5-(4-methoxyphenyl)-pent-4-en-3-ol

Guidance literature:: With sodium bis(2-methoxyethoxy)aluminium dihydride; In diethyl ether; toluene; at 0 - 20 ℃; for 12h; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1002/anie.201004072