N₂-(1,1-dimethyl-2-methylthioethyl)-3-iodo-N₁-(4-iodo-2-methylphenyl)phthalamide

Base Information

• Chemical Name: N₂-(1,1-dimethyl-2-methylthioethyl)-3-iodo-N₁-(4-iodo-2-methylphenyl)phthalamide
• CAS No.: 474557-91-0
• Molecular Formula: C₂₀H₂₂I₂N₂O₂S
• Molecular Weight: 608.282

Synonyms:N₂-(1,1-dimethyl-2-methylthioethyl)-3-iodo-N₁-(4-iodo-2-methylphenyl)phthalamide

Chemical Property of N₂-(1,1-dimethyl-2-methylthioethyl)-3-iodo-N₁-(4-iodo-2-methylphenyl)phthalamide

Chemical Property:

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Technology Process of N₂-(1,1-dimethyl-2-methylthioethyl)-3-iodo-N₁-(4-iodo-2-methylphenyl)phthalamide

There total 1 articles about N₂-(1,1-dimethyl-2-methylthioethyl)-3-iodo-N₁-(4-iodo-2-methylphenyl)phthalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

N-(1,1-dimethyl-2-methylthioethyl)-6-iodophthalic acid isoimide (866639-18-1) + 4-iodo-2-methylaniline (13194-68-8) → N2-(1,1-dimethyl-2-methylthioethyl)-3-iodo-N1-(4-iodo-2-methylphenyl)phthalamide (474557-91-0)

Guidance literature:

In acetonitrile; for 0.166667h;

Reference yield: 74.0%

N2-(1,1-dimethyl-2-methylthioethyl)-3-iodo-N1-(4-iodo-2-methylphenyl)phthalamide (474557-91-0) → N2-(1,1-dimethyl-2-methylsulfonylethyl)-3-iodo-N1-(4-iodo-2-methylphenyl)phthalamide (474557-93-2)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In chloroform; at 20 ℃; for 3h;

Reference yield: 71.0%

N2-(1,1-dimethyl-2-methylthioethyl)-3-iodo-N1-(4-iodo-2-methylphenyl)phthalamide (474557-91-0) → N2-(1,1-dimethyl-2-methylsulfinylethyl)-3-iodo-N1-(4-iodo-2-methylphenyl)phthalamide (474557-92-1)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In chloroform; at 0 - 20 ℃; for 1h;

upstream raw materials:

N-(1,1-dimethyl-2-methylthioethyl)-6-iodophthalic acid isoimide

4-iodo-2-methylaniline

Downstream raw materials:

N₂-(1,1-dimethyl-2-methylsulfonylethyl)-3-iodo-N₁-(4-iodo-2-methylphenyl)phthalamide

N₂-(1,1-dimethyl-2-methylsulfinylethyl)-3-iodo-N₁-(4-iodo-2-methylphenyl)phthalamide

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