2-azido-3,6-di-O-benzyl-2-deoxy-4-O-pentafluoropropionyl-β-D-galactopyranosyl fluoride

Base Information

• Chemical Name: 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-pentafluoropropionyl-β-D-galactopyranosyl fluoride
• CAS No.: 904700-86-3
• Molecular Formula: C₂₃H₂₁F₆N₃O₅
• Molecular Weight: 533.427

Synonyms:2-azido-3,6-di-O-benzyl-2-deoxy-4-O-pentafluoropropionyl-β-D-galactopyranosyl fluoride

Chemical Property of 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-pentafluoropropionyl-β-D-galactopyranosyl fluoride

Chemical Property:

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Technology Process of 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-pentafluoropropionyl-β-D-galactopyranosyl fluoride

There total 1 articles about 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-pentafluoropropionyl-β-D-galactopyranosyl fluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-azido-3,6-di-O-benzyl-2-deoxy-4-O-pentafluoropropionyl-D-galactopyranose → 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-pentafluoropropionyl-β-D-galactopyranosyl fluoride (904700-86-3) + 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-pentafluoropropionyl-α-D-galactopyranosyl fluoride

Guidance literature:

With 4,4'-diaminostilbene-2,2'-disulfonic acid; In dichloromethane; at -40 ℃; for 2h;

DOI:10.1016/j.carres.2006.03.011

Reference yield: 96.0%

2-azido-3,6-di-O-benzyl-2-deoxy-4-O-pentafluoropropionyl-β-D-galactopyranosyl fluoride (904700-86-3) + C83H95N9O22Si → C106H115F5N12O27Si

Guidance literature:

With bis(cyclopentadienyl)hafnium dichloride; 4 A molecular sieve; silver perchlorate; In chloroform; at 60 ℃; for 84h;

DOI:10.1016/j.carres.2006.03.011

Reference yield: 80.0%

2-azido-3,6-di-O-benzyl-2-deoxy-4-O-pentafluoropropionyl-β-D-galactopyranosyl fluoride (904700-86-3) + tert-butyldiphenylsilyl 2-azido-3,6-di-O-benzyl-2-deoxy-α-D-galactopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-β-D-galactopyranoside (904701-12-8) → tert-butyldiphenylsilyl 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-pentafluoropropionyl-D-galactopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-α-D-galactopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-β-D-galactopyranoside

Guidance literature:

With bis(cyclopentadienyl)hafnium dichloride; 4 A molecular sieve; silver perchlorate; In chloroform; at 20 ℃; for 42h;

DOI:10.1016/j.carres.2006.03.011

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