C₆₃H₉₀Cl₃N₉O₂₁

Base Information

Chemical Name:C₆₃H₉₀Cl₃N₉O₂₁
CAS No.:864875-53-6
Molecular Formula:C₆₃H₉₀Cl₃N₉O₂₁
Molecular Weight:1415.81
Hs Code.:

C<sub>63</sub>H<sub>90</sub>Cl<sub>3</sub>N<sub>9</sub>O<sub>21</sub>

Synonyms:C₆₃H₉₀Cl₃N₉O₂₁

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₆₃H₉₀Cl₃N₉O₂₁

Chemical Property:

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Technology Process of C₆₃H₉₀Cl₃N₉O₂₁

There total 28 articles about C₆₃H₉₀Cl₃N₉O₂₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 864875-47-8
(2S,3R,4R,5R,6R)-5-azido-2-(iodomethyl)-6-phenoxytetrahydro-2H-pyran-3,4-diol

: 864875-53-6
C₆₃H₉₀Cl₃N₉O₂₁

Guidance literature:: Multi-step reaction with 11 steps

1: 93 percent / pyridine

2: H₂; Et₃N / Pd/C / ethanol

3: pyridine

4: 86 percent / n-Bu₄NI; CAN / acetonitrile

5: 73 percent / Pd(OAc)2; (o-Tol)3P; Et₃N / acetonitrile / 70 °C

6: Zn; AcOH / tetrahydrofuran

7: HgCl₂; Et₃N / dimethylformamide

8: pyridine / CH₂Cl₂

9: NaN₃ / dimethylformamide

10: 73 percent / HS(CH₂)3SH; Et₃N / methanol

11: acetonitrile

With pyridine; 1.3-propanedithiol; palladium diacetate; sodium azide; ammonium cerium(IV) nitrate; hydrogen; tetra-(n-butyl)ammonium iodide; acetic acid; triethylamine; tris-(o-tolyl)phosphine; mercury dichloride; zinc; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile; 5: Heck reaction;
DOI:10.1002/anie.200500892

Reference yield:

: 864875-46-7
(2R,3R,4R,5R,6R)-5-azido-2-(hydroxymethyl)-6-phenoxytetrahydro-2H-pyran-3,4-diol

: 864875-53-6
C₆₃H₉₀Cl₃N₉O₂₁

Guidance literature:: Multi-step reaction with 13 steps

1: 81 percent / pyridine

2: 91 percent / NaI; n-Bu₄NI / 1,2-dimethoxy-ethane

3: 93 percent / pyridine

4: H₂; Et₃N / Pd/C / ethanol

5: pyridine

6: 86 percent / n-Bu₄NI; CAN / acetonitrile

7: 73 percent / Pd(OAc)2; (o-Tol)3P; Et₃N / acetonitrile / 70 °C

8: Zn; AcOH / tetrahydrofuran

9: HgCl₂; Et₃N / dimethylformamide

10: pyridine / CH₂Cl₂

11: NaN₃ / dimethylformamide

12: 73 percent / HS(CH₂)3SH; Et₃N / methanol

13: acetonitrile

With pyridine; 1.3-propanedithiol; palladium diacetate; sodium azide; ammonium cerium(IV) nitrate; hydrogen; tetra-(n-butyl)ammonium iodide; acetic acid; triethylamine; tris-(o-tolyl)phosphine; sodium iodide; mercury dichloride; zinc; palladium on activated charcoal; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile; 7: Heck reaction;
DOI:10.1002/anie.200500892

Reference yield:

: (2R,3R,4R,5R,6R)-2-(acetoxymethyl)-5-azido-6-phenoxytetrahydro-2H-pyran-3,4-diyl

: 864875-53-6
C₆₃H₉₀Cl₃N₉O₂₁

Guidance literature:: Multi-step reaction with 14 steps

1: K₂CO₃; MeOH

2: 81 percent / pyridine

3: 91 percent / NaI; n-Bu₄NI / 1,2-dimethoxy-ethane

4: 93 percent / pyridine

5: H₂; Et₃N / Pd/C / ethanol

6: pyridine

7: 86 percent / n-Bu₄NI; CAN / acetonitrile

8: 73 percent / Pd(OAc)2; (o-Tol)3P; Et₃N / acetonitrile / 70 °C

9: Zn; AcOH / tetrahydrofuran

10: HgCl₂; Et₃N / dimethylformamide

11: pyridine / CH₂Cl₂

12: NaN₃ / dimethylformamide

13: 73 percent / HS(CH₂)3SH; Et₃N / methanol

14: acetonitrile

With pyridine; 1.3-propanedithiol; methanol; palladium diacetate; sodium azide; ammonium cerium(IV) nitrate; hydrogen; tetra-(n-butyl)ammonium iodide; potassium carbonate; acetic acid; triethylamine; tris-(o-tolyl)phosphine; sodium iodide; mercury dichloride; zinc; palladium on activated charcoal; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile; 8: Heck reaction;
DOI:10.1002/anie.200500892