Technology Process of C24H37NO4S2
There total 5 articles about C24H37NO4S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
methanol; camphor-10-sulfonic acid;
In
dichloromethane;
at 0 ℃;
for 1.5h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 1H-imidazole / dichloromethane / 0.08 h / 0 °C
1.2: 0.5 h
2.1: lithium aluminium tetrahydride / tetrahydrofuran / 14 h / 0 - 60 °C
3.1: sodium hydride / N,N-dimethyl-formamide / 0.33 h / 0 °C
3.2: 4 h / 20 °C
4.1: camphor-10-sulfonic acid; methanol / dichloromethane / 1.5 h / 0 °C
With
1H-imidazole; methanol; lithium aluminium tetrahydride; camphor-10-sulfonic acid; sodium hydride;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium aluminium tetrahydride / tetrahydrofuran / 14 h / 0 - 60 °C
2.1: sodium hydride / N,N-dimethyl-formamide / 0.33 h / 0 °C
2.2: 4 h / 20 °C
3.1: camphor-10-sulfonic acid; methanol / dichloromethane / 1.5 h / 0 °C
With
methanol; lithium aluminium tetrahydride; camphor-10-sulfonic acid; sodium hydride;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;