C₂₄H₃₃N₅O₅

Base Information

Chemical Name:C₂₄H₃₃N₅O₅
CAS No.:1260090-31-0
Molecular Formula:C₂₄H₃₃N₅O₅
Molecular Weight:471.557
Hs Code.:

C<sub>24</sub>H<sub>33</sub>N<sub>5</sub>O<sub>5</sub>

Synonyms:C₂₄H₃₃N₅O₅

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Chemical Property of C₂₄H₃₃N₅O₅

Chemical Property:

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Technology Process of C₂₄H₃₃N₅O₅

There total 7 articles about C₂₄H₃₃N₅O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1260089-90-4
1-(4-(7-allyl-7-methyl-4-((S)-3-methylmorpholino)-5,7-dihydrofuro[3,4-d]pyrimidin-2-yl)phenyl)-3-ethylurea

: 1260090-31-0
C₂₄H₃₃N₅O₅

Guidance literature:: With osmium(VIII) oxide; water; 4-methylmorpholine N-oxide; In tetrahydrofuran; at 20 ℃; for 48h; Cooling with ice;

Reference yield:

: 1260090-23-0
(+/-)-7-allyl-7-methyl-5,7-dihydrofuro[3,4-d]pyrimidine-2,4(1H,3H)-dione

: 1260090-31-0
C₂₄H₃₃N₅O₅

Guidance literature:: Multi-step reaction with 4 steps

1: trichlorophosphate / 1,2-dichloro-ethane / 90 °C

2: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 1.5 h / 0 °C

3: potassium phosphate; bis(dibenzylideneacetone)-palladium⁽⁰⁾; tricyclohexylphosphine / water; acetonitrile / 90 °C

4: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / tetrahydrofuran / 48 h / 20 °C

With potassium phosphate; osmium(VIII) oxide; water; 4-methylmorpholine N-oxide; N-ethyl-N,N-diisopropylamine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; trichlorophosphate; tricyclohexylphosphine; In tetrahydrofuran; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm200215y

Reference yield:

: 1260090-18-3
ethyl 5-allyl-5-methyl-4-oxotetrahydrofuran-3-carboxylate

: 1260090-31-0
C₂₄H₃₃N₅O₅

Guidance literature:: Multi-step reaction with 6 steps

1.1: ammonium acetate / ethanol / 85 °C

2.1: pyridine / 1,2-dichloro-ethane; toluene / 2.17 h / 0 - 20 °C

2.2: 0 - 50 °C

3.1: trichlorophosphate / 1,2-dichloro-ethane / 90 °C

4.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 1.5 h / 0 °C

5.1: potassium phosphate; bis(dibenzylideneacetone)-palladium⁽⁰⁾; tricyclohexylphosphine / water; acetonitrile / 90 °C

6.1: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / tetrahydrofuran / 48 h / 20 °C

With pyridine; potassium phosphate; osmium(VIII) oxide; ammonium acetate; water; 4-methylmorpholine N-oxide; N-ethyl-N,N-diisopropylamine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; trichlorophosphate; tricyclohexylphosphine; In tetrahydrofuran; ethanol; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1021/jm200215y