1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-1-methyl-2-propylidenehydrazine

Base Information

Chemical Name:1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-1-methyl-2-propylidenehydrazine
CAS No.:1363809-24-8
Molecular Formula:C₁₇H₂₄N₂O₂
Molecular Weight:288.39
Hs Code.:

Synonyms:1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-1-methyl-2-propylidenehydrazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-1-methyl-2-propylidenehydrazine

Chemical Property:

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Technology Process of 1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-1-methyl-2-propylidenehydrazine

There total 11 articles about 1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-1-methyl-2-propylidenehydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1363807-14-0
1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-1-methylhydrazine

: 123-38-6
propionaldehyde

: 1363809-24-8
1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-1-methyl-2-propylidenehydrazine

Guidance literature:: In methanol; at 20 ℃; for 1.5h;

Reference yield:

: 314084-61-2
1-bromo-2,6-diethyl-4-methylbenzene

: 1363809-24-8
1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-1-methyl-2-propylidenehydrazine

Guidance literature:: Multi-step reaction with 6 steps

1.1: magnesium; ethylene dibromide / toluene; tetrahydrofuran / 52 h / 40 - 50 °C / Inert atmosphere

1.2: 2 h / 0 - 5 °C / Inert atmosphere

2.1: hydrazine hydrate / methanol / 4.08 h / 1 - 2 °C

3.1: toluene / 2 h / 50 °C / 100 Torr / Inert atmosphere

4.1: potassium carbonate / acetone / 1.5 h / 20 °C / Inert atmosphere

5.1: hydrogen / 5%-palladium/activated carbon / 1,2-dimethoxyethane / 8 h / 20 °C

6.1: methanol / 1.5 h / 20 °C

With hydrogen; potassium carbonate; hydrazine hydrate; magnesium; ethylene dibromide; 5%-palladium/activated carbon; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; acetone; toluene;

Reference yield:

: 1363806-98-7
ethyl 2-(2,6-diethyl-4-methylphenyl)-2-oxoacetate

: 1363809-24-8
1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-1-methyl-2-propylidenehydrazine

Guidance literature:: Multi-step reaction with 5 steps

1: hydrazine hydrate / methanol / 4.08 h / 1 - 2 °C

2: methanol / 1.5 h / 20 °C

3: potassium carbonate / N,N-dimethyl-formamide / 2.5 h / 20 °C

4: hydroxylamine / water; methanol / 17 h / 50 - 60 °C

5: methanol / 1.5 h / 20 °C

With hydroxylamine; potassium carbonate; hydrazine hydrate; In methanol; water; N,N-dimethyl-formamide;