1-Iodo-2-[2-[2-[2-[2-(2-azidoethoxy)ethoxy]ethoxy]ethoxy]ethoxy]ethane

Base Information

• Chemical Name: 1-Iodo-2-[2-[2-[2-[2-(2-azidoethoxy)ethoxy]ethoxy]ethoxy]ethoxy]ethane
• CAS No.: 936917-40-7
• Molecular Formula: C₁₂H₂₄IN₃O₅
• Molecular Weight: 417.244
• DSSTox Substance ID: DTXSID401244960
• Nikkaji Number: J2.964.344J
• Mol file: 936917-40-7.mol

Synonyms:DTXSID401244960;1-Azido-17-iodo-3,6,9,12,15-pentaoxaheptadecane;1-Iodo-2-[2-[2-[2-[2-(2-azidoethoxy)ethoxy]ethoxy]ethoxy]ethoxy]ethane;936917-40-7

Chemical Property of 1-Iodo-2-[2-[2-[2-[2-(2-azidoethoxy)ethoxy]ethoxy]ethoxy]ethoxy]ethane

Chemical Property:

• XLogP3: 1.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 7
• Rotatable Bond Count: 17
• Exact Mass: 417.07607
• Heavy Atom Count: 21
• Complexity: 255

Purity/Quality:

>98.00% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C(COCCOCCOCCOCCOCCI)N=[N+]=[N-]

Technology Process of 1-Iodo-2-[2-[2-[2-[2-(2-azidoethoxy)ethoxy]ethoxy]ethoxy]ethoxy]ethane

There total 1 articles about 1-Iodo-2-[2-[2-[2-[2-(2-azidoethoxy)ethoxy]ethoxy]ethoxy]ethoxy]ethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

triethylene glycol di-(p-toluenesulfonate) (19249-03-7) → 1-azido-17-iodo-3,6,9,12,15-pentaoxaheptadecane (936917-40-7)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydride / mineral oil / 1.5 h / 20 °C / Inert atmosphere

2: sodium iodide / N,N-dimethyl-formamide / 5 h / 50 °C / Inert atmosphere

With sodium hydride; sodium iodide; In N,N-dimethyl-formamide; mineral oil;

DOI:10.1039/c1ob05040k

Reference yield:

1-azido-17-iodo-3,6,9,12,15-pentaoxaheptadecane (936917-40-7) → C25H36F4N4O11S (1309456-99-2)

Guidance literature:

Multi-step reaction with 3 steps

1: N,N-dimethyl-formamide / 1 h / 50 °C / Inert atmosphere

2: palladium on carbon; hydrogen / methanol / 1 h / 20 °C

3: N,N-dimethyl-formamide / 2.5 h / 20 °C / Darkness; Inert atmosphere

With palladium on carbon; hydrogen; In methanol; N,N-dimethyl-formamide;

DOI:10.1039/c1ob05040k

upstream raw materials:

triethylene glycol di-(p-toluenesulfonate)

Downstream raw materials:

C₂₅H₃₆F₄N₄O₁₁S