2-(trimethylsilyl)ethyl (6-O-benzoyl-β-D-galactopyranosyl)-(1->3)-2,6-di-O-(4-methoxybenzyl)-β-D-galactopyranoside

Base Information

Chemical Name:2-(trimethylsilyl)ethyl (6-O-benzoyl-β-D-galactopyranosyl)-(1->3)-2,6-di-O-(4-methoxybenzyl)-β-D-galactopyranoside
CAS No.:1123178-54-0
Molecular Formula:C₄₀H₅₄O₁₄Si
Molecular Weight:786.946
Hs Code.:

Synonyms:2-(trimethylsilyl)ethyl (6-O-benzoyl-β-D-galactopyranosyl)-(1->3)-2,6-di-O-(4-methoxybenzyl)-β-D-galactopyranoside

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Chemical Property of 2-(trimethylsilyl)ethyl (6-O-benzoyl-β-D-galactopyranosyl)-(1->3)-2,6-di-O-(4-methoxybenzyl)-β-D-galactopyranoside

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Technology Process of 2-(trimethylsilyl)ethyl (6-O-benzoyl-β-D-galactopyranosyl)-(1->3)-2,6-di-O-(4-methoxybenzyl)-β-D-galactopyranoside

There total 1 articles about 2-(trimethylsilyl)ethyl (6-O-benzoyl-β-D-galactopyranosyl)-(1->3)-2,6-di-O-(4-methoxybenzyl)-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 613-90-1
benzoyl cyanide

: 1123178-53-9
2-(trimethylsilyl)ethyl (β-D-galactopyranosyl)-(1->3)-2,6-di-O-(4-methoxybenzyl)-β-D-galactopyranoside

: 1123178-54-0
2-(trimethylsilyl)ethyl (6-O-benzoyl-β-D-galactopyranosyl)-(1->3)-2,6-di-O-(4-methoxybenzyl)-β-D-galactopyranoside

Guidance literature:: With triethylamine; In acetonitrile; at -40 ℃; for 1.25h; Inert atmosphere;
DOI:10.1021/jm801058n

Reference yield: 47.0%

: 1123178-55-1
methyl (methyl 5-acetamido-4,7,8-tri-O-acetyl-9-azido-2-thio-3,5,9-trideoxy-D-glycero-D-galacto-2-nonulopyranosid)onate

: 1123178-54-0
2-(trimethylsilyl)ethyl (6-O-benzoyl-β-D-galactopyranosyl)-(1->3)-2,6-di-O-(4-methoxybenzyl)-β-D-galactopyranoside

: 1194454-31-3
C₅₈H₇₈N₄O₂₄Si

: 1123178-56-2
2-(trimethylsilyl)ethyl (methyl 5-acetamido-4,7,8-tri-O-acetyl-9-azido-3,5,9-trideoxy-D-glycero-α-D-galacto-2-nonulopyranosynate)-(2->3)-(6-O-benzoyl-β-D-galactopyranosyl)-(1->3)-2,6-di-O-(4-methoxybenzyl)-β-D-galactopyranoside

Guidance literature:: methyl (methyl 5-acetamido-4,7,8-tri-O-acetyl-9-azido-2-thio-3,5,9-trideoxy-D-glycero-D-galacto-2-nonulopyranosid)onate; 2-(trimethylsilyl)ethyl (6-O-benzoyl-β-D-galactopyranosyl)-(1->3)-2,6-di-O-(4-methoxybenzyl)-β-D-galactopyranoside; In acetonitrile; at 20 ℃; for 6h; Inert atmosphere; Molecular sieve;

With dimethyl(methylthio)sulfonium triflate; In acetonitrile; at 0 ℃; for 16h; Inert atmosphere; Molecular sieve;
DOI:10.1021/jm801058n