Technology Process of C35H46O8
There total 7 articles about C35H46O8 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C35H48O9;
With
2,4,6-trichlorobenzoyl chloride; triethylamine;
In
toluene;
at 20 ℃;
for 3.5h;
With
dmap;
In
toluene;
at 20 ℃;
for 4h;
DOI:10.1016/j.tet.2013.02.008
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 1H-imidazole / tetrahydrofuran / 4 h / 20 °C
2.1: sodium periodate; potassium permanganate / tert-butyl alcohol; aq. phosphate buffer / 1 h / 20 °C / pH 7.2 / Inert atmosphere
3.1: pyridine hydrogenfluoride / tetrahydrofuran / 22 h / 4 °C / Cooling
4.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 3.5 h / 20 °C
4.2: 4 h / 20 °C
With
1H-imidazole; potassium permanganate; sodium periodate; 2,4,6-trichlorobenzoyl chloride; pyridine hydrogenfluoride; triethylamine;
In
tetrahydrofuran; aq. phosphate buffer; toluene; tert-butyl alcohol;
4.1: |Yamaguchi Lactonization / 4.2: |Yamaguchi Lactonization;
DOI:10.1016/j.tet.2013.02.008
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium periodate; potassium permanganate / tert-butyl alcohol; aq. phosphate buffer / 1 h / 20 °C / pH 7.2 / Inert atmosphere
2.1: pyridine hydrogenfluoride / tetrahydrofuran / 22 h / 4 °C / Cooling
3.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 3.5 h / 20 °C
3.2: 4 h / 20 °C
With
potassium permanganate; sodium periodate; 2,4,6-trichlorobenzoyl chloride; pyridine hydrogenfluoride; triethylamine;
In
tetrahydrofuran; aq. phosphate buffer; toluene; tert-butyl alcohol;
3.1: |Yamaguchi Lactonization / 3.2: |Yamaguchi Lactonization;
DOI:10.1016/j.tet.2013.02.008
