(methyl 2-O-benzoyl-4-O-levulinoyl-3-O-methyl-α-L-idopyranosyluronate)-(1->4)-6-O-acetyl-2-O-butyl-3-O-methyl-α/β-D-glucopyranose trichloroacetimidate

Base Information

Chemical Name:(methyl 2-O-benzoyl-4-O-levulinoyl-3-O-methyl-α-L-idopyranosyluronate)-(1->4)-6-O-acetyl-2-O-butyl-3-O-methyl-α/β-D-glucopyranose trichloroacetimidate
CAS No.:1388150-90-0
Molecular Formula:C₃₅H₄₆Cl₃NO₁₆
Molecular Weight:843.106
Hs Code.:

(methyl 2-O-benzoyl-4-O-levulinoyl-3-O-methyl-α-L-idopyranosyluronate)-(1->4)-6-O-acetyl-2-O-butyl-3-O-methyl-α/β-D-glucopyranose trichloroacetimidate

Synonyms:(methyl 2-O-benzoyl-4-O-levulinoyl-3-O-methyl-α-L-idopyranosyluronate)-(1->4)-6-O-acetyl-2-O-butyl-3-O-methyl-α/β-D-glucopyranose trichloroacetimidate

Suppliers and Price of (methyl 2-O-benzoyl-4-O-levulinoyl-3-O-methyl-α-L-idopyranosyluronate)-(1->4)-6-O-acetyl-2-O-butyl-3-O-methyl-α/β-D-glucopyranose trichloroacetimidate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (methyl 2-O-benzoyl-4-O-levulinoyl-3-O-methyl-α-L-idopyranosyluronate)-(1->4)-6-O-acetyl-2-O-butyl-3-O-methyl-α/β-D-glucopyranose trichloroacetimidate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (methyl 2-O-benzoyl-4-O-levulinoyl-3-O-methyl-α-L-idopyranosyluronate)-(1->4)-6-O-acetyl-2-O-butyl-3-O-methyl-α/β-D-glucopyranose trichloroacetimidate

There total 9 articles about (methyl 2-O-benzoyl-4-O-levulinoyl-3-O-methyl-α-L-idopyranosyluronate)-(1->4)-6-O-acetyl-2-O-butyl-3-O-methyl-α/β-D-glucopyranose trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (methyl 2-O-benzoyl-4-O-levulinoyl-3-O-methyl-α-L-idopyranosyluronate)-(1->4)-6-O-acetyl-2-O-butyl-3-O-methyl-α/β-D-glucopyranose

: 545-06-2
trichloroacetonitrile

: 1388150-90-0
(methyl 2-O-benzoyl-4-O-levulinoyl-3-O-methyl-α-L-idopyranosyluronate)-(1->4)-6-O-acetyl-2-O-butyl-3-O-methyl-α/β-D-glucopyranose trichloroacetimidate

Guidance literature:: With caesium carbonate; In dichloromethane; at 0 - 20 ℃; for 1.5h;

Reference yield:

: 1388150-82-0
1,6-anhydro-2-O-butyl-3-O-methyl-4-O-(2-tetrahydropyranyl)-β-D-glucopyranose

: 1388150-90-0
(methyl 2-O-benzoyl-4-O-levulinoyl-3-O-methyl-α-L-idopyranosyluronate)-(1->4)-6-O-acetyl-2-O-butyl-3-O-methyl-α/β-D-glucopyranose trichloroacetimidate

Guidance literature:: Multi-step reaction with 8 steps

1.1: hydrogenchloride; water / methanol / 1.5 h / 0 - 20 °C

2.1: dichloromethane / 1.5 h / 20 °C / Molecular sieve; Inert atmosphere

2.2: 0.25 h / -20 °C

3.1: water; acetic acid / 1,2-dichloro-ethane / 2 h / 60 °C

4.1: sodium hydrogencarbonate; 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / tetrahydrofuran / 3.25 h / 0 - 20 °C

4.2: 16 h / 0 - 20 °C

5.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / 1,4-dioxane / 16 h / 20 °C / Inert atmosphere

6.1: trifluoroacetic acid / 16 h / 0 - 20 °C

7.1: morpholine; acetic acid / toluene / 6.25 h / 0 - 20 °C

8.1: caesium carbonate / dichloromethane / 1.5 h / 0 - 20 °C

With morpholine; hydrogenchloride; dmap; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; water; sodium hydrogencarbonate; caesium carbonate; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; 1,2-dichloro-ethane; toluene;

Reference yield:

: 1388150-83-1
1,6-anhydro-2-O-butyl-3-O-methyl-β-D-glucopyranose

: 1388150-90-0
(methyl 2-O-benzoyl-4-O-levulinoyl-3-O-methyl-α-L-idopyranosyluronate)-(1->4)-6-O-acetyl-2-O-butyl-3-O-methyl-α/β-D-glucopyranose trichloroacetimidate

Guidance literature:: Multi-step reaction with 7 steps

1.1: dichloromethane / 1.5 h / 20 °C / Molecular sieve; Inert atmosphere

1.2: 0.25 h / -20 °C

2.1: water; acetic acid / 1,2-dichloro-ethane / 2 h / 60 °C

3.1: sodium hydrogencarbonate; 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / tetrahydrofuran / 3.25 h / 0 - 20 °C

3.2: 16 h / 0 - 20 °C

4.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / 1,4-dioxane / 16 h / 20 °C / Inert atmosphere

5.1: trifluoroacetic acid / 16 h / 0 - 20 °C

6.1: morpholine; acetic acid / toluene / 6.25 h / 0 - 20 °C

7.1: caesium carbonate / dichloromethane / 1.5 h / 0 - 20 °C

With morpholine; dmap; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; water; sodium hydrogencarbonate; caesium carbonate; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In tetrahydrofuran; 1,4-dioxane; dichloromethane; 1,2-dichloro-ethane; toluene;