dichloro(1,4-diphenyl-3-diphenylphosphino-4-deuterium-1-aza-1,3-butadiene-N**1,P**3')palladium(II)

Base Information

• Chemical Name: dichloro(1,4-diphenyl-3-diphenylphosphino-4-deuterium-1-aza-1,3-butadiene-N**1,P**3')palladium(II)
• CAS No.: 301159-53-5
• Molecular Formula: C₂₇H₂₂Cl₂NPPd
• Molecular Weight: 569.77

Synonyms:dichloro(1,4-diphenyl-3-diphenylphosphino-4-deuterium-1-aza-1,3-butadiene-N**1,P**3')palladium(II)

Chemical Property of dichloro(1,4-diphenyl-3-diphenylphosphino-4-deuterium-1-aza-1,3-butadiene-N**1,P**3')palladium(II)

Chemical Property:

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Technology Process of dichloro(1,4-diphenyl-3-diphenylphosphino-4-deuterium-1-aza-1,3-butadiene-N**1,P**3')palladium(II)

There total 1 articles about dichloro(1,4-diphenyl-3-diphenylphosphino-4-deuterium-1-aza-1,3-butadiene-N**1,P**3')palladium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

((S)-1-[1-(dimethylamino)ethyl]naphthyl-C**2,N)(1,4-diphenyl-3-diphenylphosphino-4-deuterium-1-aza-1,3-butadiene-N**1,P**3')palladium(II) perchlorate + lithium chloride → dichloro(1,4-diphenyl-3-diphenylphosphino-4-deuterium-1-aza-1,3-butadiene-N**1,P**3')palladium(II) (301159-53-5)

Guidance literature:

With H₂SO₄; In water; under N2; to a soln. of complex was added concd. H2SO4, the soln. was then poured into ice and LiCl was added, the mixt. was stirred for 1 h; CH2Cl2 was added, the org. layer was sepd., the aq. layer was extd. with CH2Cl2, the combined org. layer was washed with H2O and then dried over MgSO4, the solvent was removed, the residue was recrystd. from CH2Cl2/(CH3CH2)2O; elem. anal.;

DOI:10.1021/om000416l

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