methyl 2-<<4-butyl-2-methyl-6-oxo-5-<<2'-(1H-tetrazol-5-yl)<1,1'-biphenyl>-4-yl>methyl>-1(6H)-pyrimidinyl>methyl>-3-furancarboxylate

Base Information

Chemical Name:methyl 2-<<4-butyl-2-methyl-6-oxo-5-<<2'-(1H-tetrazol-5-yl)<1,1'-biphenyl>-4-yl>methyl>-1(6H)-pyrimidinyl>methyl>-3-furancarboxylate
CAS No.:172292-58-9
Molecular Formula:C₃₀H₃₀N₆O₄
Molecular Weight:538.606
Hs Code.:

Synonyms:methyl 2-<<4-butyl-2-methyl-6-oxo-5-<<2'-(1H-tetrazol-5-yl)<1,1'-biphenyl>-4-yl>methyl>-1(6H)-pyrimidinyl>methyl>-3-furancarboxylate

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Chemical Property of methyl 2-<<4-butyl-2-methyl-6-oxo-5-<<2'-(1H-tetrazol-5-yl)<1,1'-biphenyl>-4-yl>methyl>-1(6H)-pyrimidinyl>methyl>-3-furancarboxylate

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Technology Process of methyl 2-<<4-butyl-2-methyl-6-oxo-5-<<2'-(1H-tetrazol-5-yl)<1,1'-biphenyl>-4-yl>methyl>-1(6H)-pyrimidinyl>methyl>-3-furancarboxylate

There total 8 articles about methyl 2-<<4-butyl-2-methyl-6-oxo-5-<<2'-(1H-tetrazol-5-yl)<1,1'-biphenyl>-4-yl>methyl>-1(6H)-pyrimidinyl>methyl>-3-furancarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 148564-35-6
2-{4-Butyl-2-methyl-6-oxo-5-[2'-(1-trityl-1H-tetrazol-5-yl)-biphenyl-4-ylmethyl]-6H-pyrimidin-1-ylmethyl}-furan-3-carboxylic acid methyl ester

: 172292-58-9
methyl 2-<<4-butyl-2-methyl-6-oxo-5-<<2'-(1H-tetrazol-5-yl)<1,1'-biphenyl>-4-yl>methyl>-1(6H)-pyrimidinyl>methyl>-3-furancarboxylate

Guidance literature:: With methanol; Heating;
DOI:10.1021/jm00024a008

Reference yield:

: 6947-94-0
2-methyl-3-furancarboxylic acid

: 172292-58-9
methyl 2-<<4-butyl-2-methyl-6-oxo-5-<<2'-(1H-tetrazol-5-yl)<1,1'-biphenyl>-4-yl>methyl>-1(6H)-pyrimidinyl>methyl>-3-furancarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: H₂SO₄

2: 74.5 percent / N-bromosuccinimide, α,α'-azoisobutyronitrile / CCl4 / 3 h / 70 °C

3: 1.) NaH, 2.) LiBr

4: 73 percent / MeOH / Heating

With methanol; N-Bromosuccinimide; sulfuric acid; azobisisobutyronitrile; sodium hydride; lithium bromide; In tetrachloromethane;
DOI:10.1021/jm00024a008

Reference yield:

: 6141-58-8
methyl 2-methyl-3-furancarboxylate

: 172292-58-9
methyl 2-<<4-butyl-2-methyl-6-oxo-5-<<2'-(1H-tetrazol-5-yl)<1,1'-biphenyl>-4-yl>methyl>-1(6H)-pyrimidinyl>methyl>-3-furancarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 74.5 percent / N-bromosuccinimide, α,α'-azoisobutyronitrile / CCl4 / 3 h / 70 °C

2: 1.) NaH, 2.) LiBr

3: 73 percent / MeOH / Heating

With methanol; N-Bromosuccinimide; azobisisobutyronitrile; sodium hydride; lithium bromide; In tetrachloromethane;
DOI:10.1021/jm00024a008