1,3,4-tri-O-acetyl-2-N-(benzyloxycarbonyl)-2,6-dideoxy-2-methylamino-L-glucopyranose

Base Information

Chemical Name:1,3,4-tri-O-acetyl-2-N-(benzyloxycarbonyl)-2,6-dideoxy-2-methylamino-L-glucopyranose
CAS No.:111275-50-4
Molecular Formula:C₂₁H₂₇NO₉
Molecular Weight:437.447
Hs Code.:

Synonyms:1,3,4-tri-O-acetyl-2-N-(benzyloxycarbonyl)-2,6-dideoxy-2-methylamino-L-glucopyranose

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Chemical Property of 1,3,4-tri-O-acetyl-2-N-(benzyloxycarbonyl)-2,6-dideoxy-2-methylamino-L-glucopyranose

Chemical Property:

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Technology Process of 1,3,4-tri-O-acetyl-2-N-(benzyloxycarbonyl)-2,6-dideoxy-2-methylamino-L-glucopyranose

There total 1 articles about 1,3,4-tri-O-acetyl-2-N-(benzyloxycarbonyl)-2,6-dideoxy-2-methylamino-L-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 111275-49-1
1,3,4-tri-O-acetyl-2-N-(benzyloxycarbonyl)-2,6-dideoxy-2-methylamino-6-iodo-L-glucopyranose

: 111275-50-4
1,3,4-tri-O-acetyl-2-N-(benzyloxycarbonyl)-2,6-dideoxy-2-methylamino-L-glucopyranose

Guidance literature:: With hydrogen; nickel; In ethanol; for 3h;
DOI:10.1248/cpb.34.3741

Reference yield:

: 111275-50-4
1,3,4-tri-O-acetyl-2-N-(benzyloxycarbonyl)-2,6-dideoxy-2-methylamino-L-glucopyranose

: 3,4-di-O-acetyl-2'-N-(benzyloxycarbonyl)-2,6-dideoxy-2-methylamino-L-glucopyranose

Guidance literature:: With hydrogenchloride; acetic acid;
DOI:10.1248/cpb.34.3741

Reference yield:

: 111275-50-4
1,3,4-tri-O-acetyl-2-N-(benzyloxycarbonyl)-2,6-dideoxy-2-methylamino-L-glucopyranose

: 111275-47-9,111322-21-5
1-O-(2,6-dideoxy-2-amino-β-L-glucopyranosyl)-4'-O-demethyl-1-epipodophyllotoxin

Guidance literature:: Multi-step reaction with 2 steps

1: hydrochloric acid, acetic acid

2: boron trifluoride etherate / 0.5 h / -18 °C

With hydrogenchloride; boron trifluoride diethyl etherate; acetic acid;
DOI:10.1248/cpb.34.3741