C₂₂H₂₇NO₅

Base Information

Chemical Name:C₂₂H₂₇NO₅
CAS No.:911830-79-0
Molecular Formula:C₂₂H₂₇NO₅
Molecular Weight:385.46
Hs Code.:

C<sub>22</sub>H<sub>27</sub>NO<sub>5</sub>

Synonyms:C₂₂H₂₇NO₅

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Chemical Property of C₂₂H₂₇NO₅

Chemical Property:

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Technology Process of C₂₂H₂₇NO₅

There total 6 articles about C₂₂H₂₇NO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 911830-77-8
C₂₂H₂₇NO₄

: 911830-79-0
C₂₂H₂₇NO₅

Guidance literature:: With sodium chlorite; sodium dihydrogenphosphate; In tert-butyl alcohol; at 20 ℃; for 2.5h;
DOI:10.1055/s-2006-942426

Reference yield:

: (2S,3S,1'R)-4-amino-3-O-benzyl-1,2-O-isopropylidene-5-methyl-N-(1'-phenylethyl)-6-heptene-1,2,3-triol

: 911830-79-0
C₂₂H₂₇NO₅

Guidance literature:: Multi-step reaction with 6 steps

1: 78 percent / K₂CO₃; K₃[Fe(CN)6]; hydroquinidine 1,4-phthalazinediyl diether / K₂OsO₂(OH)4 / 2-methyl-propan-2-ol; H₂O / 8 h / 20 °C

2: 99 percent / NaIO₄ / methanol; tetrahydrofuran; H₂O / 3 h / 0 °C

3: 90 percent / aq. NaClO₂; NaH₂PO₄ / 2-methyl-propan-2-ol; various solvent(s) / 2.5 h / 20 °C

4: 86 percent / diethyl ether / 0.33 h / 20 °C

5: 100 percent / H₅IO₆ / diethyl ether / 6 h / 20 °C

6: 86 percent / NaClO₂; NaH₂PO₄ / 2-methyl-propan-2-ol; various solvent(s) / 2.5 h / 20 °C

With sodium chlorite; sodium periodate; sodium dihydrogenphosphate; (DHQD)2PHAL; potassium carbonate; periodic acid; potassium hexacyanoferrate(III); potassium dioxotetrahydroxoosmate(VI); In tetrahydrofuran; methanol; diethyl ether; water; tert-butyl alcohol;
DOI:10.1055/s-2006-942426

Reference yield:

: 911830-70-1
(2S,3S,4R,5R,1'R)-4-amino-2-O-benzyl-1,2-O-isopropylidene-5-methyl-4-N-(1'-phenylethyl)heptane-1,2,3,6,7-pentol

: 911830-79-0
C₂₂H₂₇NO₅

Guidance literature:: Multi-step reaction with 5 steps

1: 99 percent / NaIO₄ / methanol; tetrahydrofuran; H₂O / 3 h / 0 °C

2: 90 percent / aq. NaClO₂; NaH₂PO₄ / 2-methyl-propan-2-ol; various solvent(s) / 2.5 h / 20 °C

3: 86 percent / diethyl ether / 0.33 h / 20 °C

4: 100 percent / H₅IO₆ / diethyl ether / 6 h / 20 °C

5: 86 percent / NaClO₂; NaH₂PO₄ / 2-methyl-propan-2-ol; various solvent(s) / 2.5 h / 20 °C

With sodium chlorite; sodium periodate; sodium dihydrogenphosphate; periodic acid; In tetrahydrofuran; methanol; diethyl ether; water; tert-butyl alcohol;
DOI:10.1055/s-2006-942426