Technology Process of 1-bromo-2,5-dioctadecyloxybenzaldehyde
There total 6 articles about 1-bromo-2,5-dioctadecyloxybenzaldehyde which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridinium chlorochromate;
In
dichloromethane;
for 4h;
Heating;
DOI:10.1021/ma0488111
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 90 percent / KOH / dimethylsulfoxide / 2 h / 20 °C
2: 73 percent / NaBr; AcOH; H2SO4 / 48 h / 100 - 110 °C
3: 99 percent / AcOH / 6 h / Heating
4: 66 percent / aq. KOH / methanol; tetrahydrofuran / 6 h / Heating
5: 61 percent / pyridinium chlorochromate / CH2Cl2 / 4 h / Heating
With
potassium hydroxide; sulfuric acid; acetic acid; pyridinium chlorochromate; sodium bromide;
In
tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide;
DOI:10.1021/ma0488111
- Guidance literature:
-
Multi-step reaction with 6 steps
1: Br2; AcOH
2: 90 percent / KOH / dimethylsulfoxide / 2 h / 20 °C
3: 73 percent / NaBr; AcOH; H2SO4 / 48 h / 100 - 110 °C
4: 99 percent / AcOH / 6 h / Heating
5: 66 percent / aq. KOH / methanol; tetrahydrofuran / 6 h / Heating
6: 61 percent / pyridinium chlorochromate / CH2Cl2 / 4 h / Heating
With
potassium hydroxide; sulfuric acid; bromine; acetic acid; pyridinium chlorochromate; sodium bromide;
In
tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide;
DOI:10.1021/ma0488111
