Triethyl-[(Z)-3-(4-nitro-phenyl)-3-oxo-propenyl]-ammonium; chloride

Base Information

• Chemical Name: Triethyl-[(Z)-3-(4-nitro-phenyl)-3-oxo-propenyl]-ammonium; chloride
• CAS No.: 109449-92-5
• Molecular Formula: C₁₅H₂₁N₂O₃*Cl
• Molecular Weight: 312.796
• Mol file: 109449-92-5.mol

Synonyms:Triethyl-[(Z)-3-(4-nitro-phenyl)-3-oxo-propenyl]-ammonium; chloride

Chemical Property of Triethyl-[(Z)-3-(4-nitro-phenyl)-3-oxo-propenyl]-ammonium; chloride

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of Triethyl-[(Z)-3-(4-nitro-phenyl)-3-oxo-propenyl]-ammonium; chloride

There total 1 articles about Triethyl-[(Z)-3-(4-nitro-phenyl)-3-oxo-propenyl]-ammonium; chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(E)-3-chloro-1-(4-nitrophenyl)-2-propenone (41037-42-7) + triethylamine (121-44-8) → triethyl-[3-(4-nitro-phenyl)-3-oxo-propenyl]-ammonium; chloride (109449-92-5)

Guidance literature:

With diethyl ether;

Reference yield: 83.0%

Triethyl-[(Z)-3-(4-nitro-phenyl)-3-oxo-propenyl]-ammonium; chloride (109449-92-5) + ethyl 2-sulfanylacetate (623-51-8) → [(Z)-3-(4-Nitro-phenyl)-3-oxo-propenylsulfanyl]-acetic acid ethyl ester (132039-29-3)

Guidance literature:

In ethanol; at 78 ℃; for 2h;

Reference yield: 80.0%

Triethyl-[(Z)-3-(4-nitro-phenyl)-3-oxo-propenyl]-ammonium; chloride (109449-92-5) + 1-mercaptopropan-2-one (24653-75-6) → (Z)-1-(4-Nitro-phenyl)-3-(2-oxo-propylsulfanyl)-propenone

Guidance literature:

In ethanol; at 78 ℃; for 1h;

upstream raw materials:

(E)-3-chloro-1-(4-nitrophenyl)-2-propenone

triethylamine

Downstream raw materials:

[(Z)-3-(4-Nitro-phenyl)-3-oxo-propenylsulfanyl]-acetic acid ethyl ester

2-acetyl-3-(p-nitrophenyl)thiophene

ethyl 3-(p-nitrophenyl)-2-thiophenecarboxylate