Technology Process of C15H9(2)H5O
There total 3 articles about C15H9(2)H5O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
boron trifluoride diethyl etherate;
In
diethyl ether;
at 20 ℃;
for 0.0166667h;
DOI:10.1021/ja058026j
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 0.168 g / mCPBA; NaHCO3 / CH2Cl2 / 0 °C
2: 102 mg / BF3*OEt2 / diethyl ether / 0.02 h / 20 °C
With
boron trifluoride diethyl etherate; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid;
In
diethyl ether; dichloromethane;
DOI:10.1021/ja058026j
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: n-BuLi / tetrahydrofuran; hexane / 1 h / 0 °C
1.2: 0.207 g / tetrahydrofuran; hexane / 2 h / 0 °C
2.1: 0.168 g / mCPBA; NaHCO3 / CH2Cl2 / 0 °C
3.1: 102 mg / BF3*OEt2 / diethyl ether / 0.02 h / 20 °C
With
n-butyllithium; boron trifluoride diethyl etherate; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; diethyl ether; hexane; dichloromethane;
DOI:10.1021/ja058026j