7-O-(4-O-p-Nitrobenzoyl-2,3,6-trideoxy-3-trifluoroacetylamido-α-L-arabino-hexopyranosyl)-ε-isorhodomycinone

Base Information

Chemical Name:7-O-(4-O-p-Nitrobenzoyl-2,3,6-trideoxy-3-trifluoroacetylamido-α-L-arabino-hexopyranosyl)-ε-isorhodomycinone
CAS No.:130320-86-4
Molecular Formula:C₃₇H₃₃F₃N₂O₁₆
Molecular Weight:818.668
Hs Code.:

Synonyms:7-O-(4-O-p-Nitrobenzoyl-2,3,6-trideoxy-3-trifluoroacetylamido-α-L-arabino-hexopyranosyl)-ε-isorhodomycinone

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Chemical Property of 7-O-(4-O-p-Nitrobenzoyl-2,3,6-trideoxy-3-trifluoroacetylamido-α-L-arabino-hexopyranosyl)-ε-isorhodomycinone

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Technology Process of 7-O-(4-O-p-Nitrobenzoyl-2,3,6-trideoxy-3-trifluoroacetylamido-α-L-arabino-hexopyranosyl)-ε-isorhodomycinone

There total 2 articles about 7-O-(4-O-p-Nitrobenzoyl-2,3,6-trideoxy-3-trifluoroacetylamido-α-L-arabino-hexopyranosyl)-ε-isorhodomycinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 21204-32-0
ε-iso-rhodomycinone

: 73891-04-0
2,3,6-tridesoxy-4-O-p-nitrobenzoyl-3-(trifluoroacetamido)-L-arabino-hex-1-enitol

: 130320-86-4
7-O-(4-O-p-Nitrobenzoyl-2,3,6-trideoxy-3-trifluoroacetylamido-α-L-arabino-hexopyranosyl)-ε-isorhodomycinone

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; In dichloromethane; acetone; at -15 ℃; for 2h;
DOI:10.1016/0008-6215(90)84241-L

Reference yield: 70.0%

: 21204-32-0
ε-iso-rhodomycinone

: 166191-09-9
1-O-tert-butyldimethylsilyl 4-O-p-nitrobenzoyl-2,3,6-trideoxy-3-trifluoroacetamido-β-L-arabino-hexopyranoside

: 130320-86-4
7-O-(4-O-p-Nitrobenzoyl-2,3,6-trideoxy-3-trifluoroacetylamido-α-L-arabino-hexopyranosyl)-ε-isorhodomycinone

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; In dichloromethane; acetone; at -35 ℃; for 6h;
DOI:10.1016/S0008-6215(00)00257-3