3-[di(tert-butyl)phosphanyl]-1-(2,6-diethylphenyl)-1H-imidazol-3-ium triflate

Base Information

Chemical Name:3-[di(tert-butyl)phosphanyl]-1-(2,6-diethylphenyl)-1H-imidazol-3-ium triflate
CAS No.:1354579-14-8
Molecular Formula:CF₃O₃S*C₂₁H₃₄N₂P
Molecular Weight:494.559
Hs Code.:

Synonyms:3-[di(tert-butyl)phosphanyl]-1-(2,6-diethylphenyl)-1H-imidazol-3-ium triflate

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Chemical Property of 3-[di(tert-butyl)phosphanyl]-1-(2,6-diethylphenyl)-1H-imidazol-3-ium triflate

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Technology Process of 3-[di(tert-butyl)phosphanyl]-1-(2,6-diethylphenyl)-1H-imidazol-3-ium triflate

There total 1 articles about 3-[di(tert-butyl)phosphanyl]-1-(2,6-diethylphenyl)-1H-imidazol-3-ium triflate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 39106-95-1
di-tert-butylphosphanylbromide

: 2926-30-9
sodium triflate

: 25364-42-5
1-(2,6-diethylphenyl)-1H-imidazole

: 1354579-14-8
3-[di(tert-butyl)phosphanyl]-1-(2,6-diethylphenyl)-1H-imidazol-3-ium triflate

Guidance literature:: In tetrahydrofuran; at 18 ℃; for 12h;
DOI:10.1016/j.tetlet.2011.11.054

Reference yield: 57.0%

: 1354579-14-8
3-[di(tert-butyl)phosphanyl]-1-(2,6-diethylphenyl)-1H-imidazol-3-ium triflate

: 1354579-07-9
3-[di(tert-butyl)phosphanyl]-1-(2,6-diethylphenyl)imidazol-2-ylidene

Guidance literature:: With sodium hexamethyldisilazane; In diethyl ether; at 0 ℃; for 0.533333h;
DOI:10.1016/j.tetlet.2011.11.054

Reference yield:

: 1354579-14-8
3-[di(tert-butyl)phosphanyl]-1-(2,6-diethylphenyl)-1H-imidazol-3-ium triflate

: 1354579-12-6
2-[di(tert-butyl)phosphanyl]-1-(2,6-diethylphenyl)-1H-imidazole

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hexamethyldisilazane / diethyl ether / 0.53 h / 0 °C

2: benzene-d6 / 3 h / 150 °C / Sealed tube

With sodium hexamethyldisilazane; In diethyl ether; benzene-d6;
DOI:10.1016/j.tetlet.2011.11.054