5-(tert-butyloxycarbonylamino)-2-[(S)-4,4-dimethyl-2-(fluoren-9-ylmethyloxycarbonylamino)pentanoylamino]terephthalic acid 1-(4-methoxybenzyl)amide

Base Information

Chemical Name:5-(tert-butyloxycarbonylamino)-2-[(S)-4,4-dimethyl-2-(fluoren-9-ylmethyloxycarbonylamino)pentanoylamino]terephthalic acid 1-(4-methoxybenzyl)amide
CAS No.:1146730-50-8
Molecular Formula:C₄₃H₄₈N₄O₉
Molecular Weight:764.876
Hs Code.:

5-(tert-butyloxycarbonylamino)-2-[(S)-4,4-dimethyl-2-(fluoren-9-ylmethyloxycarbonylamino)pentanoylamino]terephthalic acid 1-(4-methoxybenzyl)amide

Synonyms:5-(tert-butyloxycarbonylamino)-2-[(S)-4,4-dimethyl-2-(fluoren-9-ylmethyloxycarbonylamino)pentanoylamino]terephthalic acid 1-(4-methoxybenzyl)amide

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Chemical Property of 5-(tert-butyloxycarbonylamino)-2-[(S)-4,4-dimethyl-2-(fluoren-9-ylmethyloxycarbonylamino)pentanoylamino]terephthalic acid 1-(4-methoxybenzyl)amide

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Technology Process of 5-(tert-butyloxycarbonylamino)-2-[(S)-4,4-dimethyl-2-(fluoren-9-ylmethyloxycarbonylamino)pentanoylamino]terephthalic acid 1-(4-methoxybenzyl)amide

There total 1 articles about 5-(tert-butyloxycarbonylamino)-2-[(S)-4,4-dimethyl-2-(fluoren-9-ylmethyloxycarbonylamino)pentanoylamino]terephthalic acid 1-(4-methoxybenzyl)amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1146730-49-5
5-(tert-butyloxycarbonylamino)-2-[(S)-4,4-dimethyl-2-(fluoren-9-ylmethyloxycarbonylamino)pentanoylamino]terephthalic acid 1-(4-methoxybenzyl)amide 4-methyl ester

: 1146730-50-8
5-(tert-butyloxycarbonylamino)-2-[(S)-4,4-dimethyl-2-(fluoren-9-ylmethyloxycarbonylamino)pentanoylamino]terephthalic acid 1-(4-methoxybenzyl)amide

Guidance literature:: With potassium carbonate; In ethanol; water; at 50 ℃; for 2h;
DOI:10.1002/chem.200802151

Reference yield: 53.0%

: 1146730-50-8
5-(tert-butyloxycarbonylamino)-2-[(S)-4,4-dimethyl-2-(fluoren-9-ylmethyloxycarbonylamino)pentanoylamino]terephthalic acid 1-(4-methoxybenzyl)amide

: 15028-41-8
methyl 2-aminoisobutyrate hydrochloride

: 1146730-51-9
5-(tert-butyloxycarbonylamino)-2-[(S)-4,4-dimethyl-2-(fluoren-9-ylmethyloxycarbonylamino)pentanoylamino]terephthalic acid 1-(4-methoxybenzyl)amide 4-[1-(methoxycarbonyl)-1-methylethyl]amide

Guidance literature:: 5-(tert-butyloxycarbonylamino)-2-[(S)-4,4-dimethyl-2-(fluoren-9-ylmethyloxycarbonylamino)pentanoylamino]terephthalic acid 1-(4-methoxybenzyl)amide; With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 0.0166667h;

methyl 2-aminoisobutyrate hydrochloride; With benzotriazol-1-ol; triethylamine; In dichloromethane; at 80 ℃; for 48h;
DOI:10.1002/chem.200802151