C₂₅H₂₈O₃Si

Base Information

Chemical Name:C₂₅H₂₈O₃Si
CAS No.:1286210-10-3
Molecular Formula:C₂₅H₂₈O₃Si
Molecular Weight:404.581
Hs Code.:

C<sub>25</sub>H<sub>28</sub>O<sub>3</sub>Si

Synonyms:C₂₅H₂₈O₃Si

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Chemical Property of C₂₅H₂₈O₃Si

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Technology Process of C₂₅H₂₈O₃Si

There total 6 articles about C₂₅H₂₈O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1286210-43-2
C₂₃H₂₅BrO₃Si

: 7486-35-3
tri-n-butyl(vinyl)tin

: 1286210-10-3
C₂₅H₂₈O₃Si

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; at 95 ℃; for 48h; Inert atmosphere;
DOI:10.1002/anie.201007613

Reference yield:

: C₂₄H₂₅BrO₄Si

: 1286210-10-3
C₂₅H₂₈O₃Si

Guidance literature:: Multi-step reaction with 2 steps

1: methanol; sodium hydrogencarbonate / 3 h / 20 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 48 h / 95 °C / Inert atmosphere

With methanol; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydrogencarbonate; In toluene; 1: Dakin oxidation / 2: Stille coupling;
DOI:10.1002/anie.201007613

Reference yield:

: 1286210-20-5
C₂₄H₂₅BrO₃Si

: 1286210-10-3
C₂₅H₂₈O₃Si

Guidance literature:: Multi-step reaction with 3 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 48 h / 20 °C

2: methanol; sodium hydrogencarbonate / 3 h / 20 °C

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 48 h / 95 °C / Inert atmosphere

With methanol; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; toluene; 1: Dakin oxidation / 2: Dakin oxidation / 3: Stille coupling;
DOI:10.1002/anie.201007613