C₂₄H₂₇NO₃Si

Base Information

Chemical Name:C₂₄H₂₇NO₃Si
CAS No.:1435943-74-0
Molecular Formula:C₂₄H₂₇NO₃Si
Molecular Weight:405.569
Hs Code.:

C<sub>24</sub>H<sub>27</sub>NO<sub>3</sub>Si

Synonyms:C₂₄H₂₇NO₃Si

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Chemical Property of C₂₄H₂₇NO₃Si

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Technology Process of C₂₄H₂₇NO₃Si

There total 3 articles about C₂₄H₂₇NO₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1435943-90-0
C₂₇H₃₁NO₃Si

: 1435943-74-0
C₂₄H₂₇NO₃Si

Guidance literature:: With morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1002/asia.201200820

Reference yield:

: 6282-41-3
α-hydroxyphenylacetic acid allyl ester

: 1435943-74-0
C₂₄H₂₇NO₃Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-ethyl-N,N-diisopropylamine; trifluoromethylsulfonic anhydride / dichloromethane / 0.25 h / -78 °C / Inert atmosphere

1.2: 2 h / 20 °C / Inert atmosphere

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; morpholine / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

With morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; trifluoromethylsulfonic anhydride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1002/asia.201200820

Reference yield:

: 611-71-2,611-72-3,17199-29-0,90-64-2
MANDELIC ACID

: 1435943-74-0
C₂₄H₂₇NO₃Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 5 h / 20 °C / Inert atmosphere

2.1: N-ethyl-N,N-diisopropylamine; trifluoromethylsulfonic anhydride / dichloromethane / 0.25 h / -78 °C / Inert atmosphere

2.2: 2 h / 20 °C / Inert atmosphere

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; morpholine / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

With morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; trifluoromethylsulfonic anhydride; potassium carbonate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/asia.201200820