<2-benzyl-3-(tert-butylsulfonyl)propionyl>-N^im-(2,4-dinitrophenyl)histidine

Base Information

Chemical Name:<2-benzyl-3-(tert-butylsulfonyl)propionyl>-N^im-(2,4-dinitrophenyl)histidine
CAS No.:126223-02-7
Molecular Formula:C₂₆H₂₉N₅O₉S
Molecular Weight:587.61
Hs Code.:

<2-benzyl-3-(tert-butylsulfonyl)propionyl>-N<sup>im</sup>-(2,4-dinitrophenyl)histidine

Synonyms:<2-benzyl-3-(tert-butylsulfonyl)propionyl>-N^im-(2,4-dinitrophenyl)histidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of <2-benzyl-3-(tert-butylsulfonyl)propionyl>-N^im-(2,4-dinitrophenyl)histidine

Chemical Property:

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Technology Process of <2-benzyl-3-(tert-butylsulfonyl)propionyl>-N^im-(2,4-dinitrophenyl)histidine

There total 3 articles about <2-benzyl-3-(tert-butylsulfonyl)propionyl>-N^im-(2,4-dinitrophenyl)histidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 126223-04-9
N-[(S)-α-[(tert-butylsulphonyl)methyl]hydrocinnamoyl]-1-(2,4-dinitrophenyl)-L-histidine methyl ester

: 126223-02-7
<2-benzyl-3-(tert-butylsulfonyl)propionyl>-N^im-(2,4-dinitrophenyl)histidine

Guidance literature:: With hydrogenchloride; In 1,4-dioxane;

Reference yield:

: 25024-53-7
Boc-His(Dnp)-OH

: 126223-02-7
<2-benzyl-3-(tert-butylsulfonyl)propionyl>-N^im-(2,4-dinitrophenyl)histidine

Guidance literature:: Multi-step reaction with 2 steps

1: 5.5M HCl / 1,2-dimethoxy-ethane / 5 h / Ambient temperature

2: NaHCO₃ / tetrahydrofuran; ethanol / 24 h / Ambient temperature

With hydrogenchloride; sodium hydrogencarbonate; In tetrahydrofuran; 1,2-dimethoxyethane; ethanol;
DOI:10.1021/jm00081a019

Reference yield:

: 135902-06-6
(S)-2-<(tert-butylsulfonyl)methyl>-3-phenylpropionic acid succinimido ester

: 25030-55-1
1-(2,4-dinitro-phenyl)-histidine

: 126223-02-7
<2-benzyl-3-(tert-butylsulfonyl)propionyl>-N^im-(2,4-dinitrophenyl)histidine

Guidance literature:: With sodium hydrogencarbonate; In tetrahydrofuran; ethanol; for 24h; Yield given; Ambient temperature;
DOI:10.1021/jm00081a019