C₆₃H₇₄N₂O₂₅

Base Information

Chemical Name:C₆₃H₇₄N₂O₂₅
CAS No.:271248-83-0
Molecular Formula:C₆₃H₇₄N₂O₂₅
Molecular Weight:1259.28
Hs Code.:

C<sub>63</sub>H<sub>74</sub>N<sub>2</sub>O<sub>25</sub>

Synonyms:C₆₃H₇₄N₂O₂₅

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₆₃H₇₄N₂O₂₅

Chemical Property:

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Technology Process of C₆₃H₇₄N₂O₂₅

There total 11 articles about C₆₃H₇₄N₂O₂₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3554-91-4
Benzyl 2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-galactopyranoside

: 271248-83-0
C₆₃H₇₄N₂O₂₅

Guidance literature:: Multi-step reaction with 4 steps

1: 73 percent / TESOTf; molecular sieves 4 Angstroem / CH₂Cl₂ / 20 °C

2: H₂O; Et₃N / methanol / 4 °C

3: 78 percent / NIS; TfOH; molecular sieves 3 Angstroem / acetonitrile; CH₂Cl₂ / 3 h / -30 °C

4: pyridine; DMAP

With pyridine; dmap; N-iodo-succinimide; trifluorormethanesulfonic acid; 3 A molecular sieve; 4 A molecular sieve; water; triethylsilyl trifluoromethyl sulfonate; triethylamine; In methanol; dichloromethane; acetonitrile; 1: Etherification / 2: Deacetylation / 3: Etherification / 4: Acetylation;
DOI:10.1039/a908511d

Reference yield:

: 939-26-4
2-bromomethylnaphthyl bromide

: 271248-83-0
C₆₃H₇₄N₂O₂₅

Guidance literature:: Multi-step reaction with 9 steps

1: 100 percent / KOH; 18-crown-6 / tetrahydrofuran / 2 °C

2: 95 percent / AcOH; H₂O / 75 °C

3: pyridine; DMAP

4: hydrazine acetate / dimethylformamide / 2 h

5: 90 percent / DBU / CH₂Cl₂ / -10 °C

6: 73 percent / TESOTf; molecular sieves 4 Angstroem / CH₂Cl₂ / 20 °C

7: H₂O; Et₃N / methanol / 4 °C

8: 78 percent / NIS; TfOH; molecular sieves 3 Angstroem / acetonitrile; CH₂Cl₂ / 3 h / -30 °C

9: pyridine; DMAP

With pyridine; dmap; potassium hydroxide; N-iodo-succinimide; 18-crown-6 ether; trifluorormethanesulfonic acid; 3 A molecular sieve; 4 A molecular sieve; water; triethylsilyl trifluoromethyl sulfonate; hydrazinium monoacetate; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile; 1: Etherification / 2: Hydrolysis / 3: Acetylation / 4: Deacetylation / 5: Addition / 6: Etherification / 7: Deacetylation / 8: Etherification / 9: Acetylation;
DOI:10.1039/a908511d

Reference yield:

: 118977-25-6
methyl (phenyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-2-thio-D-glycerol-β-D-galactonon-2-ulopyranoside)onate

: 271248-83-0
C₆₃H₇₄N₂O₂₅

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / NIS; TfOH; molecular sieves 3 Angstroem / acetonitrile; CH₂Cl₂ / 3 h / -30 °C

2: pyridine; DMAP

With pyridine; dmap; N-iodo-succinimide; trifluorormethanesulfonic acid; 3 A molecular sieve; In dichloromethane; acetonitrile; 1: Etherification / 2: Acetylation;
DOI:10.1039/a908511d