(S)-N-(1-(3-(benzyloxy)phenyl)ethylidene)-2-methylpropane-2-sulfinamide

Base Information

Chemical Name:(S)-N-(1-(3-(benzyloxy)phenyl)ethylidene)-2-methylpropane-2-sulfinamide
CAS No.:1602681-31-1
Molecular Formula:C₁₉H₂₃NO₂S
Molecular Weight:329.463
Hs Code.:

Synonyms:(S)-N-(1-(3-(benzyloxy)phenyl)ethylidene)-2-methylpropane-2-sulfinamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-N-(1-(3-(benzyloxy)phenyl)ethylidene)-2-methylpropane-2-sulfinamide

Chemical Property:

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Technology Process of (S)-N-(1-(3-(benzyloxy)phenyl)ethylidene)-2-methylpropane-2-sulfinamide

There total 1 articles about (S)-N-(1-(3-(benzyloxy)phenyl)ethylidene)-2-methylpropane-2-sulfinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 34068-01-4
1-[3-(phenylmethoxy)phenyl]ethan-1-one

: 343338-28-3
(S)-2-methylpropane-2-sulfinamide

: 1602681-31-1
(S)-N-(1-(3-(benzyloxy)phenyl)ethylidene)-2-methylpropane-2-sulfinamide

Guidance literature:: With titanium (IV) ethoxide; In tetrahydrofuran; at 75 ℃; for 72h;

Reference yield:

: 1602681-31-1
(S)-N-(1-(3-(benzyloxy)phenyl)ethylidene)-2-methylpropane-2-sulfinamide

: 1602680-67-0
6-(3-(1-amino-1-methylethyl)phenoxy)-4-(6-methylpyridin-2-ylamino)pyridazine-3-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: trimethylaluminum / toluene; n-heptane; diethyl ether / 16.01 h / -78 - 20 °C

1.2: 3.5 h

2.1: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 18 h

3.1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 0.17 h / 0 - 20 °C

3.2: 72 h / 90 °C

With palladium 10% on activated carbon; hydrogen; trimethylaluminum; sodium hydride; In tetrahydrofuran; diethyl ether; n-heptane; N,N-dimethyl-formamide; toluene; mineral oil;

Reference yield:

: 1602681-31-1
(S)-N-(1-(3-(benzyloxy)phenyl)ethylidene)-2-methylpropane-2-sulfinamide

: 3-(1-amino-1-methylethyl)phenol

Guidance literature:: Multi-step reaction with 2 steps

1.1: trimethylaluminum / toluene; n-heptane; diethyl ether / 16.01 h / -78 - 20 °C

1.2: 3.5 h

2.1: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 18 h

With palladium 10% on activated carbon; hydrogen; trimethylaluminum; In tetrahydrofuran; diethyl ether; n-heptane; toluene;