Cis-(1S)-N-methyl-N-tert-butoxycarbonyl-6-(carboxy)-7-((methylsulphonyl)amino)-4-(3,4-dichlorophenyl)-1,2,3,4-tetrahydro-1-naphthalenamine

Base Information

Chemical Name:Cis-(1S)-N-methyl-N-tert-butoxycarbonyl-6-(carboxy)-7-((methylsulphonyl)amino)-4-(3,4-dichlorophenyl)-1,2,3,4-tetrahydro-1-naphthalenamine
CAS No.:291306-60-0
Molecular Formula:C₂₄H₂₈Cl₂N₂O₆S
Molecular Weight:543.468
Hs Code.:

Synonyms:Cis-(1S)-N-methyl-N-tert-butoxycarbonyl-6-(carboxy)-7-((methylsulphonyl)amino)-4-(3,4-dichlorophenyl)-1,2,3,4-tetrahydro-1-naphthalenamine

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Chemical Property of Cis-(1S)-N-methyl-N-tert-butoxycarbonyl-6-(carboxy)-7-((methylsulphonyl)amino)-4-(3,4-dichlorophenyl)-1,2,3,4-tetrahydro-1-naphthalenamine

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Technology Process of Cis-(1S)-N-methyl-N-tert-butoxycarbonyl-6-(carboxy)-7-((methylsulphonyl)amino)-4-(3,4-dichlorophenyl)-1,2,3,4-tetrahydro-1-naphthalenamine

There total 1 articles about Cis-(1S)-N-methyl-N-tert-butoxycarbonyl-6-(carboxy)-7-((methylsulphonyl)amino)-4-(3,4-dichlorophenyl)-1,2,3,4-tetrahydro-1-naphthalenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 291306-59-7
Cis-(1S)-N-methyl-N-tert-butoxycarbonyl-6-(methoxycarbonyl)-7-((methylsulphonyl)amino)-4-(3,4-dichlorophenyl)-1,2,3,4-tetrahydro-1-naphthalenamine

: 291306-60-0
Cis-(1S)-N-methyl-N-tert-butoxycarbonyl-6-(carboxy)-7-((methylsulphonyl)amino)-4-(3,4-dichlorophenyl)-1,2,3,4-tetrahydro-1-naphthalenamine

Guidance literature:: Cis-(1S)-N-methyl-N-tert-butoxycarbonyl-6-(methoxycarbonyl)-7-((methylsulphonyl)amino)-4-(3,4-dichlorophenyl)-1,2,3,4-tetrahydro-1-naphthalenamine; With lithium hydroxide; water; In tetrahydrofuran; at 20 - 50 ℃; for 39h;

With citric acid; In dichloromethane; water;

Reference yield: 92.0%

: 291306-60-0
Cis-(1S)-N-methyl-N-tert-butoxycarbonyl-6-(carboxy)-7-((methylsulphonyl)amino)-4-(3,4-dichlorophenyl)-1,2,3,4-tetrahydro-1-naphthalenamine

: 291305-89-0
Cis-(1S)-N-methyl-6-(carboxy)-7-((methylsulphonyl)amino)-4-(3,4-dichlorophenyl)-1,2,3,4-tetrahydro-1-naphthalenamine hydrochloride

Guidance literature:: With hydrogenchloride; In dichloromethane; at 0 ℃; for 17h;

Reference yield:

: 291306-60-0
Cis-(1S)-N-methyl-N-tert-butoxycarbonyl-6-(carboxy)-7-((methylsulphonyl)amino)-4-(3,4-dichlorophenyl)-1,2,3,4-tetrahydro-1-naphthalenamine

: 291306-76-8
tert-Butyl (1S,4S)-6-(aminocarbonyl)-4-(3,4-dichlorophenyl)-7-[(methylsulphonyl)amino]-1,2,3,4-tetrahydro-1-naphthalenyl(methyl)carbamate

Guidance literature:: With ammonium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In 1,4-dioxane; at 20 ℃; for 16h;